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A kind of pretreatment method of lignocellulose

A lignocellulose and pretreatment technology, applied in the field of bioengineering and chemical industry, can solve the problems of low conversion rate of cellulase hydrolysis, increase the amount of auxiliary materials, equipment failure, etc., to improve the recycling rate and enzymatic conversion of cellulose Rate, reduce equipment failure rate, reduce the effect of operating costs

Active Publication Date: 2020-05-12
COFCO NUTRITION & HEALTH RES INST +2
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The recovery and utilization rate of hemicellulose by dilute acid warm roasting method is high (generally 70%-85%), but the conversion rate of cellulase hydrolysis is low (generally 50%-60%), and the reaction time is long and the power is low. High cost, and sugar monomers will be derived into fermentation inhibitors such as furfural and formic acid
[0006] In addition, lignocellulosic raw materials are usually mixed with a series of impurities such as more sediment, metal objects not separated by magnetic separation, vulnerable parts dropped from mechanical rotating parts, etc. These impurities will follow the materials into subsequent equipment , it is easy to cause equipment failure, increase the maintenance workload, affect the stability of production and product quality, and at the same time, the introduction of impurities will increase the amount of auxiliary materials, and auxiliary materials will be adsorbed on the body of impurities or directly react with impurities, resulting in Increased dosage of excipients

Method used

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  • A kind of pretreatment method of lignocellulose
  • A kind of pretreatment method of lignocellulose
  • A kind of pretreatment method of lignocellulose

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0032] This example is used to illustrate the lignocellulose pretreatment method of the present invention.

[0033] Lignocellulose pretreatment methods include:

[0034] (1) 10kg of crushed lignocellulose raw material is mixed with 200kg of 1.6% by weight sulfuric acid solution for rinsing and impurity removal. The time for rinsing and wetting is 25min, and then the impurities deposited at the bottom of the rinsing and wetting device are discharged for rinsing and wetting. device, and perform draining treatment, landfill the sediment obtained from the draining treatment, recover the liquid obtained from the draining treatment and return it to the rinsing and impurity removal treatment for recycling.

[0035] (2) Extruding and dehydrating the impurity-removing material obtained by rinsing and removing impurities in step (1), so that the dry matter content of the material is 40%, obtaining 20kg of material, and returning the liquid obtained by the extruding and dehydrating proce...

Embodiment 2

[0039] This example is used to illustrate the lignocellulose pretreatment method of the present invention.

[0040] Lignocellulose pretreatment methods include:

[0041] (1) Mix 10kg of crushed lignocellulosic raw materials with 160kg of 0.97% by weight sodium hydroxide solution for rinsing and impurity removal treatment. The time for rinsing and wetting is 30min, and then the impurities deposited at the bottom of the rinsing and wetting device are discharged and rinsed Wet the device and perform draining treatment, return the sediment obtained from the draining treatment to the field, and recover the liquid obtained from the draining treatment and return it to the rinsing and impurity removal treatment for recycling.

[0042] (2) Extruding and dehydrating the impurity-removing material obtained by rinsing and removing impurities in step (1), so that the dry matter content of the material is 40%, obtaining 20kg of material, and returning the liquid obtained by the extruding an...

Embodiment 3

[0048] Lignocellulose pretreatment methods include:

[0049] (1) Mix 10 kg of pulverized lignocellulose raw materials with 250 kg of process primary water for rinsing and impurity removal treatment. The time for rinsing and wetting is 20 minutes, and then the impurities that have settled to the bottom of the rinsing and wetting device are discharged from the rinsing and wetting device, and Perform draining treatment, landfill the sediment obtained from the draining treatment, recover the liquid obtained from the draining treatment and return it to the rinsing and impurity removal treatment for recycling.

[0050] (2) Extruding and dehydrating the impurity-removing material obtained by rinsing and removing impurities in step (1), so that the dry matter content of the material is 50%, obtaining 16kg of material, and returning the liquid obtained by the extruding and dehydrating process to Recycled in rinsing and impurity removal treatment.

[0051] (3) Mix 16kg of material obta...

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Abstract

The invention relates to the field of bioengineering and the field of chemical engineering, and discloses a pre-treatment method of lignocellulose. The method comprises the step of sequentially performing rinsing impurity removal treatment, extrusion dewatering treatment and steam blasting treatment on lignocellulose raw materials, or sequentially performing rinsing impurity removal treatment, uniform mixing treatment with acid-containing or alkali-containing liquid, extrusion dewatering treatment and steam blasting treatment on the lignocellulose, wherein before the extrusion dewatering treatment, the lignocellulose raw materials are in contact with acid-containing or alkali-containing liquid in at least one treatment process. The method provided by the invention has the advantages that the hemicelluloses recovery and utilization rate and the cellulose enzymolysis conversion rate can be greatly improved; impurities can also be effectively removed; and the operation cost is reduced.

Description

technical field [0001] The invention relates to the fields of bioengineering and chemical industry, in particular to a method for pretreatment of lignocellulose. Background technique [0002] Lignocellulose pretreatment methods include chemical methods, physical methods and biological methods. The purpose is to separate its three components, cellulose, hemicellulose and lignin, to hydrolyze the hemicellulose in lignocellulose, and to make cellulose The ordered structure in the cell changes, increasing the contact area between cellulose and enzyme catalysts. [0003] The current pretreatment methods include steam explosion method, dilute acid warm baking method, ammonia fiber explosion method, carbon dioxide explosion method, wet oxidation method, peroxide method, sulfur dioxide method and other methods. However, many of these methods have not been popularized due to low raw material recovery, environmental pollution, high equipment and operating costs, and complicated opera...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C12P19/14C12P19/02
Inventor 李杰魏拥辉齐林谷立秋袁敬伟李春玲林海龙武国庆许克家张宏嘉
Owner COFCO NUTRITION & HEALTH RES INST
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