Preparation method for efficient environmental-friendly rustproof water-based metal cleaning agent

A metal cleaning agent, water-based technology, applied in the field of preparation of water-based metal cleaning agent, can solve problems such as metal corrosion, damage, pollution of the environment and human body

Inactive Publication Date: 2017-05-17
丁玉琴
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0006] The technical problem mainly solved by the present invention: aiming at the problems that various metal cleaning agents frequently used at present contain various poisonous and harmful substances, are easy to cause corrosion to more active metals, cause environmental pollution and human injury, and provide a stearic acid , oleic acid, monoethanolamine, and triethanolamine to prepare anionic surfactant organic amine fatty acid soap, which is used to remove polar dirt on metal surfaces, and combine it with starch-based dodecane, a nonionic surfactant that can effectively remove oily dirt on metal surfaces Based glycoside compound, add water-soluble polyol ether, various components in solubilized cleaning agent to promote th

Method used

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Examples

Experimental program
Comparison scheme
Effect test

example 1

[0017] First weigh 30g of rice husk ash, add 50mL of hydrochloric acid solution with a mass fraction of 10%, stir in a constant temperature water bath at 90°C for 2h at 300r / min, filter, wash the filter residue with deionized water until the washing liquid is neutral, transfer to Take it out after drying in a drying oven at 110°C to constant weight, add 240mL of 10% sodium hydroxide solution, heat in a 95°C constant temperature water bath for 2 hours, filter, add sodium hydroxide to the filtrate to adjust the solution modulus to 0.5, After reacting at 60°C for 1 hour, place it on a rotary evaporator to evaporate and concentrate to a solid content of 45%, cool to 30°C and let it stand for 2 hours, add it to a centrifuge for centrifugation, and take the precipitate and dry it in a 50°C drying oven for 1 hour , to obtain sodium metasilicate pentahydrate crystals for later use; then weigh 80g of cornstarch, add it to 150mL of ethylene glycol, stir at 300r / min for 15min, slowly add ...

example 2

[0020]First, weigh 35g of rice husk ash, add 65mL of hydrochloric acid solution with a mass fraction of 10%, stir in a constant temperature water bath at 93°C for 2.5h at 350r / min, filter, wash the filter residue with deionized water until the washing liquid is neutral, transfer Dry it in a 115°C drying oven to constant weight, take it out, add 280mL of 10% sodium hydroxide solution, heat in a 98°C constant temperature water bath for 2.5h, filter, and add sodium hydroxide to the filtrate to adjust the solution modulus to 0.6, react at 63°C for 1.5h, evaporate and concentrate on a rotary evaporator until the solid content is 50%, cool to 33°C and let it stand for 2.5h, add it to a centrifuge for centrifugation, take the precipitate and dry it at 55°C Dry in the oven for 2 hours to obtain sodium metasilicate pentahydrate crystals for later use; then weigh 90g of cornstarch, add it to 165mL of ethylene glycol, stir at 350r / min for 18min, slowly add 7mL of sulfuric acid solution wi...

example 3

[0023] First weigh 40g of rice husk ash, add 80mL of hydrochloric acid solution with a mass fraction of 10%, stir at 400r / min for 3h in a constant temperature water bath at 95°C, filter, wash the filter residue with deionized water until the washing liquid is neutral, transfer to Take it out after drying in a drying oven at 120°C to constant weight, add 320mL of 10% sodium hydroxide solution, heat in a constant temperature water bath at 100°C for 3 hours, filter, add sodium hydroxide to the filtrate to adjust the solution modulus to 0.7, After reacting at 65°C for 2 hours, place it on a rotary evaporator to evaporate and concentrate to a solid content of 55%, cool to 35°C and let it stand for 3 hours, add it to a centrifuge for centrifugation, take the precipitate and put it in a drying oven at 60°C for 3 hours , to obtain sodium metasilicate pentahydrate crystals for later use; then weigh 100g of cornstarch, add it to 180mL of ethylene glycol, stir at 400r / min for 20min, slowl...

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PUM

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Abstract

The invention discloses a preparation method for an efficient environmental-friendly rustproof water-based metal cleaning agent and belongs to the technical field of preparation of metal cleaning agents. According to the preparation method, stearic acid, oleic acid, monoethanolamine and triethanolamine generate a reaction, anionic surfactant organic amine fatty acid soap is prepared and is compouned with nonionic surfactant starch-based dodecyl glucoside, water-soluble polyol ether and a solubilizing cleaning agent are added, and all components of the water-soluble polyol ether and the solubilizing cleaning agent are capable of promoting emulsified dispersion of oil stain; and coconut oil fat diethanol amide and fatty alcohol-polyoxyethylene ether are added and serve as a hard water stabilizer, corrosion inhibitor sodium benzoate protection metal is added, washing auxiliary sodium metasilicate is added to improve the decontamination capacity and the cleaning efficiency of a surfactant, defoamer dimethyl siloxane is added after even mixing, and the efficient environmental-friendly rust-proof water-based metal cleaning agent is prepared. It is proved by the examples that the metal cleaning agent is clean and environmentally friendly, free of corrosion to metal and free of harm to the human body and the environment and has the wide future development.

Description

technical field [0001] The invention discloses a preparation method of an efficient, environment-friendly and anti-rust water-based metal cleaning agent, belonging to the technical field of metal cleaning agent preparation. Background technique [0002] In the maintenance and repair of machining, mechanical equipment, automobiles, etc., diesel oil, kerosene or gasoline are mostly used as cleaning fluids to clean parts. This not only wastes energy, but also has potential unsafe factors. If you are not careful, it may lead to a fire. In recent years, a new type of metal cleaning agent has gradually been widely used. It can replace diesel, kerosene and gasoline to clean parts, and it is cheap and safe to use. It is very suitable for mechanized cleaning operations. It can wash metal without rust spots, it is called metal cleaner. [0003] Metal cleaning agents refer to industrial cleaning agents or oil cleaning agents used to remove oil, grease, and dirt from the surface of me...

Claims

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Application Information

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IPC IPC(8): C23G1/00
CPCC23G1/00
Inventor 丁玉琴王龙薛蕾
Owner 丁玉琴
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