Preparation method of device for terahertz wave detection
A terahertz and device technology, applied in the field of detectors, can solve problems such as poor sensitivity, low radiant power of terahertz light source, narrow detection frequency, etc., and achieve the effect of improving mechanical strength
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Embodiment 1
[0055] A method for preparing a device for terahertz wave detection, comprising the following steps:
[0056] (1) Under the protection of nitrogen, mix ammonium hexachloroiridate, nickel nitrate hydrate, ammonium molybdate, ethanol and propionic acid; then reflux and stir for 5 minutes, then add ammonia water; react for 10 minutes and cool to room temperature naturally, add ethyl acetate Ester polysettling and centrifugation; washing the centrifuged precipitate with water and dispersing it in ethanol to obtain a dispersion system; then adding strontium nitrate, cobalt nitrate, and water, stirring for 10 minutes, adding samarium tricene, stirring for 1 hour, to obtain a support layer precursor;
[0057] (2) Add polyvinyl alcohol, hydrogen peroxide and iron tetraphenylporphyrin to the dispersion system, stir at 50°C for 1 hour, then add ethyl naphthoyl acetate and dibutyl phthalate, reflux and stir for 10 minutes, then Concentrate to obtain a concentrate with a solid content of ...
Embodiment 2
[0066] A method for preparing a device for terahertz wave detection, comprising the following steps:
[0067] (1) Under the protection of nitrogen, mix ammonium hexachloroiridate, nickel nitrate hydrate, ammonium molybdate, ethanol and propionic acid; then reflux and stir for 5 minutes, then add ammonia water; react for 10 minutes and cool to room temperature naturally, add ethyl acetate Ester polysettling and centrifugation; washing the centrifuged precipitate with water and dispersing it in ethanol to obtain a dispersion system; then adding strontium nitrate, cobalt nitrate, and water, stirring for 10 minutes, adding samarium tricene, stirring for 1 hour, to obtain a support layer precursor;
[0068] (2) Add polyvinyl alcohol, hydrogen peroxide and iron tetraphenylporphyrin to the dispersion system, stir at 50°C for 1 hour, then add ethyl naphthoyl acetate and dibutyl phthalate, reflux and stir for 10 minutes, then Concentrate to obtain a concentrate with a solid content of ...
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