Method for improving quality of cut stems by aspartic acid based solid-phase Maillard reaction

A technology of Maillard reaction and aspartic acid, which is applied in the field of tobacco processing, can solve the problems of short Maillard reaction time, long process time, and poor aroma enhancement effect, and achieve large-scale industrial application prospects and improve sensory perception Quality, reduce the effect of smoke irritation and miscellaneous gas

Active Publication Date: 2017-10-24
HUBEI CHINA TOBACCO IND
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Invented "a method for improving the quality of cut stems" (application number: 201410002912.2). When washing the stems, the tobacco stems are soaked or washed with a circulating protease aqueous solution, and the compound enzyme solution (compound enzyme by fruit Gelase, cellulase and xylanase) are sprayed on thick stalks and stored for more than 6 hours; additives (additives refer to amino acid solutions selected from glutamic acid, phenylalanine, aspartic acid, Proline or a combination thereof) is applied to the stalks in a ratio of ≥1%, and stored at room temperature for more than 0.5 hours, which has defects such as complex process, high process cost, and long time-consuming process, and the Maillard reaction time is short, The reaction temperature is low, there is no reaction catalyst and stabilizer, it is only 0.5h at normal temperature, the reaction is not sufficient, and the aroma-enhancing effect of the Maillard reaction product is not good; invented "a processing method for improving the quality of cut stems" (application number: 201510041600.7 ), first extract the tobacco stem or stem piece with alcohol solution, and then add the alcohol extract back to the shredded stem made of the tobacco stem or stem piece, and wash the tobacco stem with acid hydrolysis and enzymatic hydrolysis macromolecules (like pectin, protein, etc.) and other compounds that are unfavorable to tobacco smoking, but the alcohol crude extract of tobacco stems still has the defects of high irritation, high concentration, obvious miscellaneous gas, and insufficient aroma; In the silk online production process, the method and application of aspartic acid, asparagine and reducing sugar / complex sugar source solid-phase Maillard reaction to improve the quality of cut stems have not been reported yet.

Method used

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  • Method for improving quality of cut stems by aspartic acid based solid-phase Maillard reaction
  • Method for improving quality of cut stems by aspartic acid based solid-phase Maillard reaction

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Embodiment 1

[0029] A method for improving the quality of cut stems by aspartic acid solid-phase Maillard reaction, comprising the following steps:

[0030] (1) raw material preparation: aspartic acid and mannose (molar ratio is 3:1) as solid-phase Maillard reaction substrate, account for 0.05% of the cut stem quality, reaction catalyst is ammonium acetate, ascorbic acid (mass ratio is 1:1), the catalyst mass accounts for 0.25% of the Maillard reaction substrate mass; the mass ratio of water to the Maillard reaction substrate is 2:1;

[0031] (2) Solid-phase Maillard reaction in the shredded stem feeding process: add water, aspartic acid, and mannose at 65°C in sequence according to the ratio of raw materials in the above step 1), and stir thoroughly until they are completely dissolved, then add the reaction catalyst (ammonium acetate, ascorbic acid), mix evenly, evenly spray on the shredded stems, make the moisture content of the shredded stems reach 30%, and carry out solid-phase Maillar...

Embodiment 2

[0036] A method for improving the quality of cut stems by aspartic acid solid-phase Maillard reaction, comprising the following steps:

[0037] (1) Raw material preparation: amino acid (aspartic acid and asparagine, molar ratio 1:1) and fermented coconut extract are used as solid-phase Maillard reaction substrate, account for 0.12% of stem shredded mass, described amino acid and The mass ratio of fermented coconut extract is 2.8:1, and reaction catalyst is decanaldehyde, ascorbic acid (mass ratio is 1:1), and catalyst quality accounts for 0.3% of Maillard reaction substrate quality; Water and Maillard reaction substrate The mass ratio is 2.5:1;

[0038] (2) Solid-phase Maillard reaction in the shredded stem feeding process: add water at 72°C, amino acids, and fermented coconut extract according to the ratio of raw materials in the above step 1) in turn, stir thoroughly until completely dissolved, then add the reaction catalyst, Mix evenly, spray evenly on the shredded stems, ...

Embodiment 3

[0044] A method for improving the quality of cut stems by aspartic acid solid-phase Maillard reaction, comprising the following steps:

[0045] (1) Raw material preparation: Amino acid (aspartic acid and asparagine are compounded at a molar ratio of 0.5:1) and complex sugar source as solid-phase Maillard reaction substrate, accounting for 0.2% of the cut stem mass, the compound Sugar source is the mixture (mass ratio of 1:1) of rhamnose and fermented coconut extract, the mass ratio of described amino acid and complex sugar source is 3:1, and reaction catalyst is ammonium acetate, ammonium bicarbonate (mass ratio is 1:1), the catalyst mass accounts for 0.5% of the Maillard reaction substrate mass; the mass ratio of water to the Maillard reaction substrate is 4:1;

[0046] (2) Solid-phase Maillard reaction in the shredded stem feeding process: add water at 80°C, amino acids, and complex sugar sources according to the ratio of raw materials in the above step 1) in sequence, and s...

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Abstract

The invention aims to provide a method for improving quality of cut stems by aspartic acid based solid-phase Maillard reaction. According to the method, in the charging production procedure of cut stems, water solution containing amino acids(aspartic acid and asparagine) and reducing sugar or complex carbohydrate source and reaction catalyst at a certain ratio is sprayed to cut stems; in the online process of the cut stems, aspartic acid based solid-phase Maillard reaction is carried out; thus, type and content of aroma components of the cut stems are increased, curing fragrance is enhanced, smoke stimulation and offensive odor are reduced, smoke is purified, smoking flavor is improved, organoleptic quality of the cut stems is improved, the cut stems processed by the method have appearance close to the high-quality cut tobacco, and the method needs mild processing conditions which are easy to realize.

Description

technical field [0001] The invention relates to the field of tobacco processing, in particular to a method for improving the quality of cut stems by aspartic acid solid-phase Maillard reaction. Background technique [0002] Tobacco is a plant of the genus Nicotiana in the family Solanaceae. The tobacco stem is the thick and hard vein of the tobacco leaf, accounting for about 25-30% of the leaf weight. Tobacco stems are by-products of the tobacco industry and are mostly disposed of at present. my country is a big tobacco country, and hundreds of thousands of tons of tobacco stem resources are discarded every year, which not only causes environmental pollution, but also wastes natural resources. Studies have shown that the types of components contained in tobacco stems are basically the same as those of tobacco leaves. Shredded stems have the characteristics of low tar and nicotine content and good filling performance. They are one of the main fillers in cigarette leaf formu...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): A24B3/12C11B9/00
CPCA24B3/12C11B9/0003
Inventor 魏敏陈义坤宋旭艳叶明樵李冉胡素霞黄龙夏秋冬潘曦郭国宁
Owner HUBEI CHINA TOBACCO IND
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