A kind of denitrification catalyst anti-heavy metal deposition and preparation method thereof
A denitration catalyst, anti-heavy metal technology, applied in metal/metal oxide/metal hydroxide catalysts, chemical instruments and methods, physical/chemical process catalysts, etc., can solve the imbalance of active centers, instability, and easy deposition of heavy metals Activity and other issues, to achieve the effect of uniform dispersion, stable catalyst activity, and high catalyst performance
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Embodiment 1
[0038] will contain TiO 2 100g of titanyl sulfate is dissolved in sulfuric acid solution to form TiO 2 For a 35g / L solution, add MoO 3 A total of 3.5g of ammonium paramolybdate solution, after ultrasonic vibration for 2 hours, gradually add ammonia water to adjust the pH value to 9.5, after the precipitation is complete, filter and wash; then the washed material is made of deionized water and 0.5g squash powder to make the water content For a 50% slurry, add V 2 o 5 A total of 0.9g of ammonium metavanadate solution was stirred and ultrasonically oscillated for 1.5h. After direct drying, it was roasted at 620°C for 8h; after roasting, the powder was mixed with MoO 3 A total of 1.0 g of ammonium molybdate solution was used to make a slurry with a water content of 30%, and after stirring, 0.8 g of turnip powder was added, stirred for 40 min, sealed and left for 24 h, dried, and roasted at 620°C for 8 h to obtain a denitrification catalyst. The fresh catalyst obtained above an...
Embodiment 2
[0042] will contain TiO 2 100g of titanyl sulfate is dissolved in sulfuric acid solution to form TiO 2 For 30g / L solution, add MoO 3 A total of 3.5g of ammonium molybdate solution was ultrasonically oscillated for 1.5h and then gradually added ammonia water to adjust the pH value to 10. After the precipitation was complete, filter and wash; For a 50% slurry, add V 2 o 5 A total of 0.9g of ammonium metavanadate solution was stirred and ultrasonically oscillated for 1.5h. After direct drying, it was roasted at 600°C for 8h; after roasting, the powder was mixed with MoO 3 A total of 0.5g of ammonium molybdate solution was used to make a slurry with a water content of 35%, and after stirring, 0.6g of turnip powder was added, stirred for 30 minutes, sealed and left for 16 hours, dried, and roasted at 600°C to obtain a denitration catalyst. The fresh catalyst obtained above and the catalyst after high-temperature mixing with the catalytic cracking waste catalyst containing heavy...
Embodiment 3
[0046] will contain TiO 2 100g of metatitanic acid is dissolved in sulfuric acid solution to form TiO-containing 2 For 30g / L solution, add MoO 3 A total of 2.5g of ammonium molybdate solution, after ultrasonic vibration for 1h, gradually add ammonia water to adjust the pH value to 9.5, after the precipitation is complete, filter and wash; then the washed material is made of deionized water and 0.3g scallop powder with a water content of 45% slurry, add V 2 o 5 A total of 0.6g of ammonium metavanadate solution was stirred and ultrasonically oscillated for 1h. After direct drying, it was roasted at 550°C for 6h; after roasting, the powder was mixed with MoO 3 A total of 0.8g of ammonium molybdate solution was prepared into a slurry with a water content of 30%. After stirring, 0.7g of scallop powder was added, stirred for 30min, sealed and left for 20h, dried, and roasted at 550°C to obtain a denitrification catalyst. The fresh catalyst obtained above and the catalyst after h...
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