High-efficient detergent for electronic product
A technology of electronic products and cleaning agents, applied in the field of cleaning agents, can solve the problems that affect the yield, performance and reliability of devices, the cleaning ability needs to be further improved, and the production cost of cleaning agents is high, so as to avoid excessive prices, use safety, and Inexpensive effect
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Embodiment 1
[0026] A high-efficiency cleaning agent for electronic products is made of the following raw materials in parts by weight:
[0027]
[0028] The preparation method of described fluorine-containing amphoteric surfactant, comprises the steps:
[0029] 1) Dissolve 100 g of N-tris(hydroxymethyl)methyl-2-aminoethanesulfonic acid in 400 g of acetonitrile, and add 200 g of 1-bromooctadecane therein, stir and react at 40° C. for 6 hours, and then pass Rotary steaming, washing 5 times with ether, and rotary steaming again to obtain the intermediate product;
[0030] 2) 90 g of the intermediate product prepared in step 1) was dissolved in 150 g of deionized water, and then 45 g of sodium hydroxide and 36 g of tetrabutylammonium bromide were added thereto, and stirred at room temperature for 0.5 hours, and then added 75g of perfluorodecane bromide, reflux and stir at 70°C for 1 hour, cool down after the reaction, extract with dichloromethane, wash 3 times with water, take the organic...
Embodiment 2
[0032] A high-efficiency cleaning agent for electronic products is made of the following raw materials in parts by weight:
[0033]
[0034] The preparation method of described fluorine-containing amphoteric surfactant, comprises the steps:
[0035] 1) Dissolve 100 g of N-tris(hydroxymethyl)methyl-2-aminoethanesulfonic acid in 500 g of ether, and add 220 g of 1-bromohexadecane to it, stir and react at 43°C for 7 hours, then pass Rotary steaming, washing with ether 6 times, rotary steaming again to obtain the intermediate product;
[0036] 2) 90 g of the intermediate product prepared in step 1) was dissolved in 160 g of deionized water, then 55 g of sodium hydroxide and 38 g of tetrabutylammonium bromide were added thereto, and stirred at room temperature for 1 hour, and then added 80g perfluorooctyl bromide, refluxed and stirred at 75°C for 17 hours, cooled after the reaction, extracted with dichloromethane, washed 4 times with water, dried the organic layer with anhydrous...
Embodiment 3
[0038] A high-efficiency cleaning agent for electronic products is made of the following raw materials in parts by weight:
[0039]
[0040] The preparation method of described fluorine-containing amphoteric surfactant, comprises the steps:
[0041] 1) 100 g of N-tris(hydroxymethyl)methyl-2-aminoethanesulfonic acid was dissolved in 550 g of ethyl acetate, and 280 g of 1-chlorohexadecane was added thereto, and the reaction was stirred at 50° C. for 7 hours, Then by rotary evaporation, washed 6 times with ether, and rotary evaporation again to obtain the intermediate product;
[0042] 2) 90 g of the intermediate product prepared in step 1) was dissolved in 170 g of deionized water, and then 49 g of sodium hydroxide and 39 g of tetrabutylammonium bromide were added thereto, and stirred at room temperature for 0.9 hours, and then added 86g perfluorodecane bromide, reflux and stir at 79°C for 19 hours, cool down after the reaction, extract with dichloromethane, wash 5 times wit...
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