Anticorrosion and antifouling type coating resin and method for preparing same
A coating and resin technology, applied in the field of anti-corrosion and anti-fouling type coating resin and its preparation, can solve the problems of difficult anti-corrosion and anti-fouling performance of coatings, and achieve the effects of good anti-fouling effect, good anti-corrosion ability and good anti-corrosion effect.
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Embodiment 1
[0018] Dissolve 0.6 kg of N-methylol acrylamide, 0.09 kg of sodium bisulfite, and 0.15 kg of sodium bicarbonate in 30.0 kg of deionized water. After all dissolved, add 42.0 kg of vinylidene chloride and 7.5 kg of methacrylic acid at room temperature. Methyl acrylate, 2.5 kg ethyl acrylate, 8.0 kg butyl acrylate, 8.5 kg 2-ethylhexyl acrylate, 1.5 kg acrylic acid, fully stirred to obtain mixed solution A; 0.2 kg N-methylol acrylamide was dissolved in 10.0 kg of deionized water, after all dissolved, add 25.0 kg of triethylsilyl acrylate, 5.0 kg of triisopropylsilyl methacrylate, and stir to obtain mixed solution B.
[0019] The reactor was evacuated and filled with nitrogen for three times, the temperature was adjusted to 25 °C, 15.0 kg of deionized aqueous solution containing 0.35 kg of ammonium persulfate and 0.07 kg of sodium bisulfite was added, and mixed solution A was added dropwise to the reaction within 3.5 h. In the device, the constant temperature reaction was completed...
Embodiment 2
[0021] Dissolve 0.8 kg of N-methylol acrylamide, 0.09 kg of sodium bisulfite, and 0.15 kg of sodium bicarbonate in 35.0 kg of deionized water. After all dissolved, add 42.0 kg of vinylidene chloride and 7.5 kg of methacrylic acid at room temperature. Methyl acrylate, 2.5 kg ethyl acrylate, 8.0 kg butyl acrylate, 8.5 kg 2-ethylhexyl acrylate, 1.5 kg acrylic acid, fully stirred to obtain mixed solution A; 0.2 kg N-methylol acrylamide was dissolved in 10.0 kg of deionized water, after all dissolved, add 25.0 kg of triethylsilyl acrylate, 5.0 kg of triisopropylsilyl methacrylate, and stir to obtain mixed solution B.
[0022] The reactor was evacuated and filled with nitrogen for three times, the temperature was adjusted to 25 °C, 20.0 kg of deionized aqueous solution containing 0.35 kg of ammonium persulfate and 0.07 kg of sodium bisulfite was added, and mixed solution A was added dropwise to the reaction within 3.5 h. In the device, the constant temperature reaction was completed...
Embodiment 3
[0024]Dissolve 0.8 kg of N-methylol acrylamide, 0.09 kg of sodium bisulfite, and 0.15 kg of sodium bicarbonate in 35.0 kg of deionized water. After all dissolved, add 38.0 kg of vinylidene chloride and 7.5 kg of methacrylic acid at room temperature. Methyl acrylate, 2.5 kg ethyl acrylate, 10.0 kg butyl acrylate, 10.5 kg 2-ethylhexyl acrylate, 1.5 kg acrylic acid, fully stirred to obtain mixed solution A; 0.2 kg N-methylol acrylamide was dissolved in 10.0 kg deionized water, after all dissolved, add 15.0 kg triethylsilyl acrylate, 5.0 kg trimethylsilyl methacrylate, 5.0 kg triisopropylsilyl acrylate, 5.0 kg trimethyl methacrylate isopropylsilyl ester, and stir to obtain mixed solution B.
[0025] The reactor was evacuated and filled with nitrogen for three times, the temperature was adjusted to 30 °C, 20.0 kg of deionized aqueous solution containing 0.35 kg of ammonium persulfate and 0.07 kg of sodium bisulfite was added, and mixed solution A was added dropwise to the reaction ...
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