Photocatalyst hydrosol with high catalytic degradation performance and its production process
A technology of catalytic degradation and production process, applied in the field of photocatalyst, can solve the problems of limited catalytic activity and practical use conditions, inability of electron holes to migrate in time, and inability to achieve catalytic effect, etc., to improve photocatalytic properties, excellent electrical properties, Reduce the effect of reducing efficiency
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Embodiment 1
[0033] The production process of photocatalyst hydrosol with high catalytic degradation performance comprises the following steps: add 1g sodium hexametaphosphate to 200g water, stir at 80 rpm for 10 minutes to obtain a mixed solution; add 5g titanium dioxide to the mixed solution, and continue to stir at 80 rpm Stir for 15 minutes per minute; then add 6g of 20% hydrogen peroxide solution in mass fraction, shear and emulsify for 30 minutes at 5000 rpm, and leave it for 12 hours to obtain an emulsion; add 0.6g acetylacetone to the emulsion, and continue to Stir at 80 rpm for 10 minutes, then adjust the pH to 7 with 1% hydrochloric acid or 1% sodium hydroxide aqueous solution by mass fraction to obtain the photocatalyst hydrosol with high catalytic degradation performance.
[0034] Use a pipette to pipette 0.5mL of the photocatalyst hydrosol with high catalytic degradation performance of Example 1 into a beaker, add water to make up to 400mL, ultrasonically treat for 20 minutes, ...
Embodiment 2
[0037] The production process of photocatalyst hydrosol with high catalytic degradation performance comprises the following steps: add 1g of sodium hexametaphosphate to 200g of water, stir at 80 rpm for 10 minutes to obtain a mixed solution; add 4g of titanium dioxide and 1g of molybdic acid to the mixed solution Bismuth, continue to stir with 80 rpm for 15 minutes; then add 6g of hydrogen peroxide solution with a mass fraction of 20%, shear and emulsify with 5000 rpm for 30 minutes, and leave it for 12 hours to obtain an emulsion; add 0.6 g acetylacetone, continue to stir at 80 rpm for 10 minutes, then adjust the pH to 7 with 1% hydrochloric acid or 1% aqueous sodium hydroxide solution by mass fraction to obtain the photocatalyst hydrosol with high catalytic degradation performance.
[0038] The preparation process of the bismuth molybdate is as follows: 4.85g bismuth nitrate pentahydrate and 0.97g sodium molybdate dihydrate are added to 400mL deionized water, after stirring f...
Embodiment 3
[0042] The production process of photocatalyst hydrosol with high catalytic degradation performance comprises the following steps: add 1g sodium hexametaphosphate to 200g water, stir at 80 rpm for 10 minutes to obtain a mixed solution; add 4g titanium dioxide and 1g selenium loading to the mixed solution Bismuth molybdate, continue to stir with 80 rpm for 15 minutes; then add 6g of hydrogen peroxide solution with a mass fraction of 20%, shear and emulsify with 5000 rpm for 30 minutes, and leave it for 12 hours to obtain an emulsion; Add 0.6g acetylacetone, continue stirring at 80 rpm for 10 minutes, then adjust the pH to 7 with 1% hydrochloric acid or 1% aqueous sodium hydroxide solution by mass fraction to obtain the photocatalyst hydrosol with high catalytic degradation performance.
[0043] The preparation process of the described selenium-loaded bismuth molybdate is as follows: 4.85g bismuth nitrate pentahydrate, 0.97g sodium molybdate dihydrate and 0.25g selenium powder ar...
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