A kind of method adopting graphene oxide Pickering emulsion to construct ammonium dinitramide coating layer
A technology of ammonium dinitramide and Pickering emulsion, applied in chemical instruments and methods, nitrated acyclic/alicyclic/heterocyclic amine explosive composition, inorganic chemistry, etc., can solve the thickness of cross-linked polymer coating layer It is difficult to control the shape and shape, reduce the moisture absorption of ammonium dinitramide, and affect the contact of ammonium dinitramide, so as to achieve significant barrier properties, reduce hygroscopicity, and increase the energy release rate.
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Examples
Embodiment 1
[0022] This embodiment provides a kind of method adopting graphene oxide Pickering emulsion to construct ammonium dinitramide coating layer, and this method specifically comprises the following steps:
[0023] Step 1: Surface modification of graphene oxide
[0024] Mix 0.1 g of graphene oxide with 50 ml of deionized water, and disperse by ultrasonic to obtain a stable graphene oxide suspension. Dissolve 0.001g of dodecylamine in 50ml of ethanol, put the above two solutions in a three-necked flask and mix them, stir at 90°C for 2h, and reflux the reaction system to obtain a precipitated reaction product. The reaction precipitate was separated from the dispersion medium through a filter membrane, and the filtered product was re-added into 50 ml of ethanol, ultrasonically dispersed for 10 minutes, and the mixed solution was filtered and dried to obtain a precipitated reaction product. The above process was repeated 5 times to fully remove physically adsorbed dodecylamine, and th...
Embodiment 2
[0032] This embodiment provides a method of using graphene oxide Pickering emulsion to construct an ammonium dinitramide coating layer. Steps 3 and 4 of this method are the same as those in Example 1, except for steps 1 and 2.
[0033] Step 1: Surface modification of graphene oxide
[0034]0.3 g of graphene oxide was mixed with 100 ml of deionized water, and dispersed by ultrasonic to obtain a stable graphene oxide suspension. Dissolve 0.002g of octadecylamine in 50ml of ethanol, put the above solution in a three-necked flask, stir at 90°C for 2h, and reflux the reaction system to obtain a precipitated reaction product. The reaction precipitate was separated from the dispersion medium through a filter membrane, and the filtered product was re-added into 50 ml of ethanol, ultrasonically dispersed for 10 minutes, and the mixed solution was filtered and dried to obtain a precipitated reaction product. The above process was repeated 5 times to fully remove the physically adsorbed...
Embodiment 3
[0038] This embodiment provides a method of using graphene oxide Pickering emulsion to construct an ammonium dinitramide coating layer. Steps 3 and 4 of this method are the same as those in Example 1, except for steps 1 and 2.
[0039] Step 1: Surface modification of graphene oxide
[0040] Mix 0.1 g of graphene oxide with 100 ml of deionized water, and disperse by ultrasonic to obtain a stable graphene oxide suspension. Dissolve 0.01 g of cyclohexylamine in 50 ml of ethanol, put the above solution in a three-necked flask, stir at 90° C. for 2 h, and reflux the reaction system to obtain a precipitated reaction product. The reaction precipitate was separated from the dispersion medium through a filter membrane, and the filtered product was re-added into 50 ml of ethanol, ultrasonically dispersed for 10 minutes, and the mixed solution was filtered and dried to obtain a precipitated reaction product. The above process was repeated 5 times to fully remove the physically adsorbed ...
PUM
Abstract
Description
Claims
Application Information
- R&D Engineer
- R&D Manager
- IP Professional
- Industry Leading Data Capabilities
- Powerful AI technology
- Patent DNA Extraction
Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic, Popular Technical Reports.
© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap|About US| Contact US: help@patsnap.com