Preparation method of lipophilic and hydrophobic magnetic polystyrene-polyurethane composite sponge
A polyurethane sponge, lipophilic and hydrophobic technology, applied in separation methods, chemical instruments and methods, alkali metal compounds, etc., can solve the problems of high heat resistance requirements of raw material foam, difficult to control the reaction process, unfavorable production and application, etc., to achieve durable Low thermal requirements, high oil-water selectivity, good elasticity
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Embodiment 1
[0031] Example 1: Preparation of lipophilic and hydrophobic magnetic polystyrene-polyurethane composite sponge
[0032] Weigh 150 mg of nano-iron tetroxide and 30 ml of absolute ethanol into a small beaker, and sonicate for 2 min to make the system evenly dispersed. Cut the polyurethane sponge into a size of 1 cm × 1 cm × 3 cm, then take a piece and add it to the beaker, and continue to sonicate for 10 min. Then, the sponge was taken out and placed in an oven with a temperature of 60° C. to dry for 2 hours to obtain a magnetic polyurethane sponge.
[0033] Measure 6 mL of styrene and 0.3 mL of divinylbenzene in turn and mix them uniformly in a quartz tube by ultrasonic for 2 min. The above-mentioned dried magnetic polyurethane sponge is immersed in the solution, protected by nitrogen, and irradiated with a high-pressure mercury lamp for 14 h. Finally, the sponge was thoroughly washed with toluene, ethyl acetate and ethanol in turn, and dried in an oven at a temperature of 60°...
Embodiment 2
[0037] Example 2: Preparation of lipophilic and hydrophobic magnetic polystyrene-polyurethane composite sponge
[0038] Weigh 150 mg of nano-iron tetroxide and 30 ml of absolute ethanol into a small beaker, and sonicate for 2 min to make the system evenly dispersed. Cut the polyurethane sponge into a size of 1 cm × 1 cm × 3 cm, then take a piece and add it to the beaker, and continue to sonicate for 10 min. Then, the sponge was taken out and placed in an oven with a temperature of 60° C. to dry for 2 hours to obtain a magnetic polyurethane sponge.
[0039] Measure 6 mL of styrene and 0.1 mL of divinylbenzene in turn and mix them uniformly in a quartz tube by ultrasonic for 2 min. Take the above-mentioned dried magnetic polyurethane sponge and immerse it in the solution, protect it with nitrogen, and irradiate it with a high-pressure mercury lamp for 14 hours. Finally, the sponge was thoroughly washed with toluene, ethyl acetate and ethanol in turn, and dried in an oven at a t...
Embodiment 3
[0041] Example 3: Preparation of lipophilic and hydrophobic magnetic polystyrene-polyurethane composite sponge
[0042] Weigh 150 mg of nano-iron tetroxide and 30 ml of absolute ethanol into a small beaker, and sonicate for 2 min to make the system evenly dispersed. Cut the polyurethane sponge into a size of 1 cm × 1 cm × 3 cm, then take a piece and add it to the beaker, and continue to sonicate for 10 min. Then, the sponge was taken out and placed in an oven with a temperature of 60° C. to dry for 2 hours to obtain a magnetic polyurethane sponge.
[0043] Measure 6 mL of styrene and 0.5 mL of divinylbenzene in turn and mix them uniformly by ultrasonic for 2 min in a quartz tube. Take the above-mentioned dried magnetic polyurethane sponge and immerse it in the solution, protect it with nitrogen, and irradiate it with a high-pressure mercury lamp for 14 hours. Finally, the sponge was thoroughly washed with toluene, ethyl acetate and ethanol in turn, and dried in an oven at a tem...
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