Green and environment-friendly wool composite fiber and refining method and application thereof

A composite fiber, green and environmental protection technology, applied in fiber processing, animal fiber, improved hand fiber, etc., can solve the problems of poor surface smoothness of thinned fibers, pollute the environment, and reduce mechanical properties, and avoid slippage and permeability. Good, good affinity

Inactive Publication Date: 2020-10-09
合肥必更赢科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

CN 103820991 B A method for modifying the surface of wool by catalytic oxidation. The aqueous dispersion of iron oxide nanoparticles is sprayed on the wool fibers so that the iron oxide nanoparticles are attached to the surface of the wool fibers, and then H 2 o 2 Solution catalysis, protease treatment, so that the surface scale structure is corroded and destroyed, and the descaling effect is achieved; CN102677450 B is a method for surface modification of wool, by using nano-TiO 2 Particles (Anatase TiO 2 Nanoparticles) are attached to wool and treated with ultraviolet light for photocatalytic treatment and protease treatment, so that the scale structure on the wool surface is partially corroded and destroyed; but the above two are not only difficult to control the degree of stripping, but also the mechanical properties of wool fiber decrease significantly
[0006] CN 105780447 B A method for modifying wool surface scales in a micro-water system. By preparing microcapsules containing sodium hydroxide, the corrosion of sodium hydroxide on wool is limited to only occur on the wool surface, so as to corrode the wool scale structure, although the use of chlorination is avoided. The problems caused by the descaling method, but a large amount of organic materials are introduced, and the surface gloss of the wool fiber is poor after corrosion
Although the existing wool stretching and thinning technology can use relatively thick wool fibers to produce thinner fibers, it is easy to generate a large amount of waste liquid and pollute the environment. At the same time, the surface smoothness of the thinned fibers is poor, and the mechanical properties drop significantly.

Method used

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  • Green and environment-friendly wool composite fiber and refining method and application thereof
  • Green and environment-friendly wool composite fiber and refining method and application thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0039] A method for thinning green and environment-friendly wool composite fibers, comprising the steps of:

[0040] S1. Mix 10kg keratin, 2kg lecithin, and 2kg tetraethyl orthosilicate evenly to obtain a premix; send the premix to a nano-impact mill for grinding, the speed of the nano-impact mill is 1500r / min, and the power is 4.5kW , the grinding temperature is 20°C, zirconia balls are used as the grinding medium, and the mass ratio of the premix to the grinding medium is 0.1:10 to obtain an environmentally friendly penetrant;

[0041] 10kg lanolic acid is dissolved in 10kg ethanol to obtain the aid of dissolving lanolic acid;

[0042] Dissolve 6kg of environmentally friendly penetrating agent in 40kg of ethanol aqueous solution with a mass fraction of 60%, stir evenly at a low temperature of 10°C, then immerse the wool top in it to increase the weight of the wool top to 164%, and then send it into the above-mentioned dissolved wool acid additive for use The weight of the w...

Embodiment 2

[0049] A method for thinning green and environment-friendly wool composite fibers, comprising the steps of:

[0050] S1. Mix 20kg keratin, 1kg lecithin, and 4kg tetraethyl orthosilicate evenly to obtain a premix; send the premix to a nano-impact mill for grinding. The speed of the nano-impact mill is 1000r / min, and the power is 5kW. The grinding temperature is 10°C, zirconia balls are used as the grinding medium, and the mass ratio of premix and grinding medium is 1:10 to obtain an environmentally friendly penetrant;

[0051] 6kg lanolic acid is dissolved in 20kg ethanol to obtain the aid of dissolving lanolic acid;

[0052] Dissolve 2kg of environmentally friendly penetrating agent in 60kg of ethanol aqueous solution with a mass fraction of 50%, stir evenly at a low temperature of 16°C, then immerse the wool top in it to increase the weight of the wool top to 160%, and then send it into the above-mentioned dissolved wool acid additive for use The weight of the wool top is in...

Embodiment 3

[0059] A method for thinning green and environment-friendly wool composite fibers, comprising the steps of:

[0060] S1, 12kg keratin, 1.8kg lecithin, and 2.5kg tetraethyl orthosilicate are mixed uniformly to obtain a premix; the premix is ​​sent to a nano-impact mill for grinding, and the speed of the nano-impact mill is 1400r / min, and the power is 4.6kW, the grinding temperature is 17°C, using zirconia balls as the grinding medium, and the mass ratio of the premix to the grinding medium is 0.2:10 to obtain an environmentally friendly penetrant;

[0061] 9kg lanolic acid is dissolved in 12kg ethanol to obtain the aid of dissolving lanolic acid;

[0062] Dissolve 5kg of environmentally friendly penetrating agent in 45kg of ethanol aqueous solution with a mass fraction of 57%, stir evenly at 12°C at low temperature, then immerse the wool top in it to increase the weight of the wool top to 163%, and then send it into the above-mentioned dissolved wool acid additive for use The ...

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Abstract

The invention discloses a refining method of green and environment-friendly wool composite fiber. The refining method comprises the following steps that an environment-friendly penetrating agent is dissolved in ethanol water, low-temperature uniform stirring is conducted, wool tops are immersed in the solution, the solution is sent into a wool acid dissolving auxiliary, the solution is taken out,lifted and subjected to standing, redundant liquid is removed, air drying is conducted, and pretreated wool fiber is obtained; and a reinforced viscose solution is sent into an impregnation tank, thepretreated wool fiber is added for ultrasonic treatment, then under extrusion and traction of a clamping roller, the reinforced viscose solution uniformly coats the pretreated wool fiber, the pretreated wool fiber is sent into a coagulating bath for coagulation, cleaning and drafting are conducted, the pretreated wool fiber is sent into a milk protein fiber spinning solution, and the green and environment-friendly wool composite fiber is obtained through curing, drafting, drying and shaping. According to the refining method, a previous technology is broken through, the fiber can reach the fineness of a common refining technology, the mechanical property of the fiber is excellent, and the surface smoothness is high; and a preparation containing available chlorine or chemical agents such assodium pyrosulfite and sodium hydrogen sulfite are not adopted for treatment, and the refining method is safe, environmentally friendly and free of environmental pollution.

Description

technical field [0001] The invention relates to the technical field of wool fiber refinement, in particular to a green and environment-friendly wool composite fiber and its refinement method and application. Background technique [0002] Wool is a high-grade textile fiber material commonly used in the manufacture of textile products such as suits, fashion and knitted sweaters. However, the surface of wool has a special structure - the scale layer, which will cause felting of wool products during use, change the size and shape of the garment, and affect the appearance and performance of the garment; at the same time, the structure of the scale layer is tight, The brightness of wool products is insufficient, and the handle is not smooth and soft enough. [0003] With the continuous development of science and technology, people's requirements for the performance of fibers and their textiles are constantly improving, and textile products are developing towards high-level and hi...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): D06M15/15D06M11/79D06M13/144D06M15/07D06M11/38D06M13/123D06M11/55D06M11/56D06M101/12
CPCD06M11/38D06M11/55D06M11/56D06M11/79D06M13/123D06M13/144D06M15/07D06M15/15D06M2101/12D06M2200/50
Inventor 严春兰
Owner 合肥必更赢科技有限公司
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