A kind of polymetallic surface protective agent and its preparation method and application

A surface protectant, multi-metal technology, applied in the field of water circulation system, can solve the problem of high requirements for circulating water, and achieve the effect of preventing fine leakage, preventing scaling and avoiding damage

Active Publication Date: 2022-07-19
烟台康恩环保科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] Therefore, the technical problem to be solved by the present invention is to overcome the defect that the corrosion inhibitors in the prior art have high requirements for circulating water, thereby providing a multi-metal surface protective agent and its preparation method and application

Method used

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  • A kind of polymetallic surface protective agent and its preparation method and application
  • A kind of polymetallic surface protective agent and its preparation method and application
  • A kind of polymetallic surface protective agent and its preparation method and application

Examples

Experimental program
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Effect test

Embodiment 1

[0057] The present embodiment provides a kind of polymetallic surface protective agent, and its preparation method is as follows:

[0058] Preparation of film formers:

[0059] 5kg benzotriazole was dissolved in 5.5kg ethanol to obtain a mixed solution for subsequent use;

[0060] 25kg deionized water is added in the reactor and heated to 60 ℃ with stirring, then add 15kg undecanedioic acid, 10kg dodecanedioic acid, 12kg gluconic acid and 15kg benzoic acid, be warming up to 90 ℃ after adding, add 15kg of triethanolamine and 3kg of ethanolamine, and continue to stir for 0.5h: then add the above mixed solution, heat up to 110°C and stir for 1.5h, and then naturally drop to room temperature to obtain the film-forming agent for later use.

[0061] Preparation of occlusive agent:

[0062] After mixing 30kg of deionized water and 10kg of ammonium citrate uniformly, add 20kg of sebacic acid and 10kg of adipic acid at 80°C, then heat up to 88°C and stir for 30min; continue to add 15...

Embodiment 2

[0070] The present embodiment provides a kind of polymetallic surface protective agent, and its preparation method is as follows:

[0071] Preparation of film formers:

[0072] 10kg of benzotriazole was dissolved in 10kg of ethanol to obtain a mixed solution for subsequent use;

[0073] 20kg deionized water was added to the reactor and heated to 60°C with stirring, then 20kg of undecanedioic acid, 15kg of dodecanedioic acid, 15kg of gluconic acid and 6kg of benzoic acid were added, and the temperature was raised to 80°C after adding. 20kg of triethanolamine and 8kg of ethanolamine, and continue to stir for 1.5h: then add the above mixed solution, heat up to 120°C and stir for 2.5h, and then naturally drop to room temperature to obtain the film-forming agent for use.

[0074] Preparation of occlusive agent:

[0075]After mixing 20kg of deionized water and 15kg of ammonium citrate uniformly, add 25kg of sebacic acid and 15kg of adipic acid at 85°C, then heat up to 90°C and sti...

Embodiment 3

[0083] The present embodiment provides a kind of polymetallic surface protective agent, and its preparation method is as follows:

[0084] Preparation of film formers:

[0085] 8kg benzotriazole was dissolved in 7.2kg ethanol to obtain a mixed solution for subsequent use;

[0086] 16kg deionized water was added to the reactor and heated to 60°C with stirring, then 10kg of undecanedioic acid, 20kg of dodecanedioic acid, 8kg of gluconic acid and 10kg of benzoic acid were added, and the temperature was raised to 100°C after adding. 10kg of triethanolamine and 5kg of ethanolamine, and continue to stir for 1.0h: then add the above mixed solution, heat up to 130°C and stir for 2.0h, and then naturally drop to room temperature to obtain the film-forming agent for later use.

[0087] Preparation of occlusive agent:

[0088] After mixing 25kg of deionized water and 5kg of ammonium citrate uniformly, add 22kg of sebacic acid and 20kg of adipic acid at 75°C, then heat up to 85°C and st...

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Abstract

The invention provides a multi-metal surface protective agent and a preparation method and application thereof. The multi-metal surface protective agent comprises the following raw materials in parts by weight: 15-21 parts of a sealing agent, 43-55 parts of a film-forming agent, and 9-5 parts of a catalyst 15 parts and 17-23 parts of pH regulator; wherein, the raw materials of the film-forming agent include organic acids, alcohol amine compounds, benzotriazole and deionized water; the raw materials of the sealing agent include organic dibasic acids , alcohol amine compounds, ammonium citrate and deionized water; the catalyst includes citric acid and lactic acid; the pH adjuster includes methyl benzotriazole and triethylamine. The polymetallic surface protective agent provided by the invention can be applied to the circulating water system, has no requirement on the water quality in the water circulating system, is suitable for water quality such as deionized water, soft water, groundwater and surface water, and has strong resistance to hard water, good The reserve alkalinity and the performance of acid and alkali resistance and high temperature resistance.

Description

technical field [0001] The invention relates to the technical field of water circulation systems, in particular to a multi-metal surface protective agent and a preparation method and application thereof. Background technique [0002] With the rapid development of economy and the rapid increase of population, water shortage has become an important factor restricting my country's economic construction and development. In my country, a large amount of water resources are used and consumed in industrial circulating water and urban heating circulating water. However, because water contains colloids, suspended solids, soluble salts such as calcium, magnesium, potassium and other oxidizing substances and dissolved gases, In the process of application, the circulating water inevitably produces scaling (calcium carbonate, calcium sulfate, barium sulfate, etc.), and at the same time, the problems of bacteria breeding and corrosion under the scale are also more prominent. Therefore, it ...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C23F11/10C02F5/12C02F1/66C02F103/06C02F103/02
CPCC23F11/10C02F5/12C02F1/66C02F2103/06C02F2103/02C02F2303/08
Inventor 赵桂琳金栋王同泽赵玉刚宋兆桐
Owner 烟台康恩环保科技有限公司
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