A compound antibacterial agent for preventing and controlling plant diseases
A compound antibacterial and medicament technology, applied in the direction of plant growth regulators, fungicides, biocides, etc., can solve the problems of high drug residues and can not meet the needs of plant pest control, etc., to achieve high bacterial efficiency, mild reaction conditions, Environmentally friendly effect
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Embodiment 1
[0021] Embodiment 1: Preparation of compound antibacterial agent
[0022] Mix component A and component B uniformly at a weight ratio of 1:4, and then dissolve with a small amount of DMSO as a stock solution.
Embodiment 2
[0023] Embodiment 2: the antibacterial property of compound antibacterial agent to canker sore citrus
[0024] Experimental strain: Canker sorrel citrus.
[0025] The experimental operation steps are as follows:
[0026] (1) Dilute the stock solution of compound antibacterial agent prepared in Example 1 with PBS solution to a final concentration of 330, 100, 33, 10, 3.3, 1, 0.33, 0.1, 0.033 μM, and then use a pipette to pipette each Concentration drug 20 μl, added to a 96-well transparent plate. The same volume of PBS solution was used as blank control.
[0027] (2) Draw 200 μl of bacterial solution (10 6 CFU / ml) was added to each dosing hole, and the solar simulator (wavelength 295-2500 nM, power 80 mW / cm 2 ) for 1 min, the light dose is 4.8 J / cm 2, and then use sterile PBS to dilute each group into different concentration gradients, the dilution gradients are 10×, 100×, 1000× and 10000×, 100000×, take 100 μl and smear it on the pre-configured bacterial culture plate, a...
Embodiment 3
[0032] Embodiment 3: minimum inhibitory concentration of composite antimicrobial agent
[0033] (1) Dilute the compound antibacterial agent with a concentration of 744 μg / ml with NB medium to a final concentration of 372, 186, 93, 46.5, 23.3, 11.7, 5.7, 2.91, 1.44, 0.72, 0.36 μg / ml. Dilute 100 μl, 4000 μg / ml copper sulfate or copper hydroxide stock solution with fresh NB medium to 2000, 1000, 500, 250, 125, 62.5, 31.25, 15.6, 7.8, 3.9 and 1.96 μg / ml The concentration was the positive control. The same volume of PBS solution was used as blank control. Use a pipette gun to pipette 100 μl of each drug concentration into a 96-well plate.
[0034] (2) Draw 100 μl of fresh bacterial solution (10 6 CFU / ml) into each dosing well, and then use a solar simulator (wavelength 295-2500 nM, power 80 mW / cm 2 ) for 1 min, the light dose is 4.8 J / cm 2 .
[0035] (3) After irradiation, continue to culture at 28°C and 200 rpm for 24 hours, the minimum inhibitory concentration of the compo...
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