Preparation method of plant antibacterial, antiviral, skin-care and health-care cellulose fibers

A technology of cellulose fiber and cellulose A, applied in the direction of cellulose/protein conjugated rayon, cellulose/protein rayon chemical post-treatment, fiber chemical characteristics, etc., can solve the problem of affecting the functionality of fibers or fabrics , loss, easy loss and other problems, to achieve the effect of good skin care and health care functions

Active Publication Date: 2021-01-12
潍坊欣龙生物材料有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The active ingredients of the functional components (tea pigments or tea polyphenols or catechins) used in this patent are basically water-soluble, basically without protection or simple adsorption protection, and are not suitable for wet processing of cellulose fibers. Spinning, there is a serious problem of loss in the subsequent spinning process, which affects the functionality of the fiber
[0010] Chinese patent 200810025069.4 (a tea cellulose fiber production process) and Chinese patent 201410282478.8 (a green tea fiber fabric) are two patented technologies that pre-process tea raw materials Pulp, and then go through the cellulose fiber production process to prepare related fibers. The production process is long. Most of the functional components in tea are damaged by strong acid and alkali, which affects the functionality of fibers or fabrics.
[0016] Collagen is a biological polymer that plays a role in combining tissues in animal cells. It is the most abundant protein in the human body and is rich in the Glycine, proline, hydroxyproline and other amino acids can improve immune function, activate cell function, activate muscles and bones, prevent skin aging, remove wrinkles, and have good skin care and health care functions, but alone
[0017] Collagen added to the spinning dope, there is also the problem of easy loss

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0044] A preparation method of plant-based antibacterial, antiviral, skin care and health care cellulose fiber whose specification is 1.33dtex*38mm is as follows:

[0045] 1. Preparation of collagen solution

[0046] Prepare a 2.0mol / L urea solution, add collagen with a molecular weight of 110kD to the prepared urea solution at a mass fraction of 8.0%, and dissolve at 85°C for 1.5h to obtain collagen with a falling ball viscosity of 15s lysate.

[0047] 2. Preparation of tea polyphenol dispersion

[0048] Tea polyphenols (purchased from Xi'an Zelang Biotechnology Co., Ltd.) were added to deionized water at 35°C and pH=7, stirred and dissolved for 30 minutes to prepare a tea polyphenols dispersion with a mass fraction of 10% tea polyphenols.

[0049] 3. Preparation of blended spinning stock solution

[0050] Using cellulose pulp as raw material, the cellulose spinning stock solution was prepared through the conventional viscose preparation process. The dissolving solution i...

Embodiment 2

[0057] A preparation method of plant-based antibacterial, antiviral, skin care and health care cellulose fibers with a specification of 1.56dtex*38mm is as follows:

[0058] 1. Preparation of collagen solution

[0059] Prepare a 2.8mol / L urea solution, add collagen with a molecular weight of 175kD to the prepared urea solution at a mass fraction of 10.5%, and dissolve at 82°C for 2.0h to obtain collagen with a falling ball viscosity of 21s lysate.

[0060] 2. Preparation of tea polyphenol dispersion

[0061] Add tea polyphenols (purchased from Xi'an Zelang Biotechnology Co., Ltd.) into deionized water at 41°C and pH=7, start stirring and dissolving for 39 minutes, and prepare a tea polyphenol dispersion with a mass fraction of 12.5% ​​tea polyphenols.

[0062] 3. Preparation of blended spinning stock solution

[0063] Using cellulose pulp as raw material, the cellulose spinning stock solution was prepared through the conventional viscose preparation process. The dissolving...

Embodiment 3

[0070] A kind of preparation method of plant antibacterial antiviral, skin care and health care cellulose fiber whose specification is 1.67dtex*38mm is as follows:

[0071] 1. Preparation of collagen solution

[0072] Prepare a 3.5mol / L urea solution, add collagen with a molecular weight of 235kD to the prepared urea solution at a mass fraction of 12.6%, heat up to 76°C and dissolve for 2.5h to obtain collagen with a falling ball viscosity of 25s lysate.

[0073] 2. Preparation of tea polyphenol dispersion

[0074] Tea polyphenols (purchased from Xi'an Zelang Biotechnology Co., Ltd.) were added to deionized water at 46°C and pH=7, stirred and dissolved for 43 minutes, and a tea polyphenol dispersion with a mass fraction of 15.6% of tea polyphenols was prepared.

[0075] 3. Preparation of blended spinning stock solution

[0076] Using cellulose pulp as raw material, the cellulose spinning stock solution was prepared through the conventional viscose preparation process. Its c...

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Abstract

The invention provides a preparation method of plant antibacterial, antiviral, skin-care and health-care cellulose fibers. The preparation method is characterized by comprising the steps of preparingof a blended spinning stock solution, spinning and aftertreatment. Tea polyphenol and zinc elements are used for endowing the fibers with excellent antibacterial and antiviral functions, meanwhile, operation is assisted by the skin-care and health-care functions of collagen, so that the prepared functional cellulose fibers have antibacterial, antiviral, skin-care and health-care functions, the inhibition rate on staphylococcus aureus is larger than or equal to 92.6%, the inhibition rate on escherichia coli is larger than or equal to 93.8%, the inhibition rate on candida albicans is larger thanor equal to 90.3%, the inactivation rate on influenza A viruses is larger than or equal to 85.6%, the inactivation rate on influenza B viruses is larger than or equal to 86.2%, and the inactivation rate on herpes viruses is larger than or equal to 82.8%. The fibers contain multiple kinds of amino acid trace elements, and therefore good skin-care and health-care functions are achieved.

Description

technical field [0001] The invention belongs to the technical field of functional regenerated cellulose fibers, and specifically relates to a kind of tea polyphenol with antibacterial and antiviral functions, zinc element and collagen for skin care and health care as raw materials, and is used for adding before spinning and post-processing. , thereby preparing plant-based antibacterial, antiviral, skin care and health care cellulose fibers and a preparation method thereof. Background technique [0002] In recent years, the textile industry has launched many fibers and textiles with health care and medical functions that are beneficial to human health and environmental protection, and have achieved gratifying results, with huge market potential. Because cellulose fiber products have the advantages of moisture absorption, good air permeability, comfortable wearing, and natural degradation, they have made great progress in health care and medical functions in recent years, amon...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): D01F8/02D01F1/10D01F11/02
CPCD01F8/02D01F1/103D01F11/02Y02A50/30
Inventor 李昌垒刘长军颜晶秦翠梅刘乐吴亚红李君宝
Owner 潍坊欣龙生物材料有限公司
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