Diamond surface modification method
A surface modification, diamond technology, applied in the direction of diamond, chemical instruments and methods, metal material coating technology, etc., can solve the problems of unfavorable protection of diamond strong binding force, inability to form a complete film layer, thick surface coating thickness, etc. Achieve strong binding force, slow down the rate of grain growth, and reduce the effect of interface thermal resistance
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
Embodiment 1
[0037] like figure 1 Shown, the present invention comprises the steps:
[0038] Step 1: Weigh 1.5g chromium powder, 3g lithium chloride, 2g sodium chloride, 2.5g potassium chloride and 1g sodium fluoride respectively, put the weighed materials into the mixing tank, add zirconia balls, ball mill 12 hours.
[0039]Step 2: Put the ball-milled material into the crucible, put the crucible into the tube furnace, and put Ar and H into the tube furnace 2 Mixture of Ar and H 2 H in the mixture 2 The volume percentage is 15%, and the temperature is raised to 800°C at a heating rate of 5°C / min and kept for 120min. When the end temperature drops to room temperature, stop the gas supply, take out the crucible and grind and sieve the reaction product (180 mesh screen) , to obtain abrasives.
[0040] Step 3: Select diamond particles of MDB8 type; diamond particle size: 70-80 μm; clean and dry the selected diamond particles; weigh 100g of diamond particles and put them in a 10% NaOH solu...
Embodiment 2
[0047] The present invention comprises the steps:
[0048] Step 1: Select and weigh 1.5g titanium powder, 2g sodium chloride, 2.5g potassium chloride, 3g lithium chloride and 1g sodium fluoride, put the weighed materials into the mixing tank, add zirconia grinding balls, Ball mill for 12 hours.
[0049] Step 2: Put the ball-milled material into the crucible, put the crucible into the tube furnace, set the heating curve of the tube furnace, feed Ar gas, and heat up from room temperature to 800 °C at a heating rate of 3 °C / min After 120 minutes, when the operation is over and the temperature drops below 100°C, the Ar gas is turned off, the crucible is taken out, and the reaction product is ground and sieved (180-mesh sieve) to obtain ground material.
[0050] Step 3: select diamond particles of MDB8 type; diamond particle size: 70-80 μm; clean and dry the selected diamond particles; prepare a mass concentration of , weigh 100g of diamond particles and put them in a mass concent...
Embodiment 3
[0054] Step 1: Weigh 1g Ti powder, 1.5g lithium chloride, 0.8g sodium chloride, 1.5g potassium chloride and 0.2g sodium fluoride respectively, put the weighed materials into the mixing tank, and add zirconia grinding balls , Ball milling for 3 hours.
[0055] Step 2: Put the ball-milled material into the crucible, put the crucible into the tube furnace, and put Ar and H into the tube furnace 2 Mixture of Ar and H 2 H in the mixture 2 The volume percentage is 15%, with the heating rate of 1 °C / min, the temperature is raised to 700 ° C for 240 min, and when the end temperature drops to room temperature, the gas supply is stopped, the crucible is taken out, and the reaction product is ground and sieved (180 mesh screen). Obtain grind.
[0056] Step 3: Select MDB8 type diamond particles; diamond particle size: 3-40μm; clean and dry the selected diamond particles; weigh 100g of diamond particles and put them in a 10% NaOH solution, wash for 10min, take out and distill water Rep...
PUM
| Property | Measurement | Unit |
|---|---|---|
| particle diameter | aaaaa | aaaaa |
| size | aaaaa | aaaaa |
| size | aaaaa | aaaaa |
Abstract
Description
Claims
Application Information
Login to View More