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Novel double-layer film coated magnetic conductive alloy powder, preparation method and application

A technology of alloy powder and double-layer film, applied in the field of material processing, can solve the problems of rapid growth of dental calculus, difficult removal of irritants, etc., and achieve the effect of complete shape, good mechanical properties and biocompatibility, and good combination.

Active Publication Date: 2022-04-12
JILIN UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0002] At present, the method of cleaning teeth in the world is mainly the crown polishing method, specifically, the tooth surface is polished at a low speed by rubber cups and polishing paste, or the tooth surface is polished by supragingival and subgingival sandblasting, but due to the different shapes of the tooth surface and the root Due to the existence of anatomical structures, it is difficult to remove the irritants inside the teeth and in the crevices of the teeth. Observed by optical microscope and scanning electron microscope, there are often deep scratches on the surface of cleaned teeth, which are easy for plaque to adhere and The formation of calculus nuclei, which will lead to rapid growth of dental calculus, leading to periodontal inflammation

Method used

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  • Novel double-layer film coated magnetic conductive alloy powder, preparation method and application
  • Novel double-layer film coated magnetic conductive alloy powder, preparation method and application
  • Novel double-layer film coated magnetic conductive alloy powder, preparation method and application

Examples

Experimental program
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Effect test

Embodiment 1

[0029] Hydroxyapatite / magnesium-iron double-layer film-coated iron-chromium alloy powder I, and its preparation method includes:

[0030] (1) Take 5.75g magnesium nitrate and 3.03g ferric nitrate as solute, measure 25mL deionized water as solvent with graduated cylinder, make Mg in the solution 2+ with Fe 3+ The ion ratio is 3:1, stir until the solute is completely dissolved in the solvent to obtain solution A; take 1.92g sodium hydroxide and 1.69g sodium carbonate as the solute, and use a graduated cylinder to measure 100mL deionized water as the solvent, so that the OH in the solution - and CO 3 2- The ion ratio is 3:1, stir until the solute is completely dissolved in the solvent, and obtain solution B; add solution B to solution A, and keep stirring until the pH of the mixed solution is 10, and obtain suspension C;

[0031](2) Take the iron-chromium alloy powder, put it into absolute ethanol and ultrasonically clean it, after cleaning, put it in a blast drying oven at 60...

Embodiment 2

[0040] Hydroxyapatite / magnesium-iron bimetallic oxide double-layer film-coated iron-chromium alloy powder II, and its preparation method includes:

[0041] (1) Take 3.04g magnesium chloride and 2.03g ferric chloride as solute, measure 25mL deionized water as solvent with graduated cylinder, make Mg in the solution 2+ with Fe 3+ The ion ratio is 2:1, stir until the solute is completely dissolved in the solvent, and obtain solution A; take 1.92g sodium hydroxide and 1.69g sodium carbonate as the solute, and use a graduated cylinder to measure 100mL deionized water as the solvent, so that the OH in the solution - and CO 3 2- The ion ratio is 3:1, stir until the solute is completely dissolved in the solvent, and obtain solution B; add solution B to solution A, and keep stirring until the pH of the mixed solution is 10, and obtain suspension C;

[0042] (2) Take the iron-chromium alloy powder, put it into absolute ethanol and ultrasonically clean it, after cleaning, put it in a ...

Embodiment 3

[0047] Hydroxyapatite / magnesium-iron bimetallic oxide double-layer coating iron-nickel alloy powder III, its preparation method comprises:

[0048] (1) Take 5.75g magnesium nitrate and 3.03g ferric nitrate as solute, measure 25mL deionized water as solvent with graduated cylinder, make Mg in the solution 2+ with Fe 3+ The ion ratio is 3:1, stir until the solute is completely dissolved in the solvent to obtain solution A; take 2.8g of potassium hydroxide and 3.46g of potassium carbonate as the solute, and use a graduated cylinder to measure 100mL of deionized water as the solvent, so that the OH in the solution - and CO 3 2- The ion ratio is 1:1, stir until the solute is completely dissolved in the solvent, and obtain solution B; add solution B to solution A, and keep stirring until the pH of the mixed solution is 9, and obtain suspension C;

[0049] (2) Take the iron-nickel alloy powder, put it into absolute ethanol for ultrasonic cleaning, after cleaning, put it in a blast...

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Abstract

The invention provides novel double-layer film coated magnetic conductive alloy powder as well as a preparation method and application thereof. The preparation method of the double-layer film coated magnetic conductive alloy powder comprises the following steps: taking magnetic conductive alloy powder as a matrix, preparing a magnesium-iron layered double-metal hydroxide on the surface of the matrix by using a hydrothermal synthesis method to serve as a middle layer, and then preparing a hydroxyapatite film layer on the outermost layer by using a sol-gel method, so as to obtain the double-layer film coated magnetic conductive alloy powder. And then the magnetic conductive alloy powder coated with the hydroxyapatite / magnesium-iron bimetal oxide double-layer film is obtained through sintering, wherein the magnetic conductive alloy powder coated with the double-layer film has excellent mechanical properties. Cell experiments prove that the magnetic conductive powder coated with the double-layer film is non-toxic and has good biocompatibility, and can be used for cleaning teeth under a magnetic control condition, specifically, the magnetic conductive powder moves relative to a tooth crown under the action of a magnetic field, the tooth crown is polished, and the tooth crown is cleaned. The tooth cleaning device can be used for comprehensively cleaning tooth surfaces, adjacent surface gaps between teeth and pit, groove and point gaps on the tooth surfaces and effectively removing bacterial plaque.

Description

technical field [0001] The invention belongs to the field of material processing, and in particular relates to a novel double-layer film-coated magnetic permeable alloy powder, a preparation method and an application. Background technique [0002] At present, the method of cleaning teeth in the world is mainly the crown polishing method, specifically, the tooth surface is polished at a low speed by rubber cups and polishing paste, or the tooth surface is polished by supragingival and subgingival sandblasting, but due to the different shapes of the tooth surface and the root Due to the existence of anatomical structures, it is difficult to remove the irritants inside the teeth and in the crevices of the teeth. Observed by optical microscope and scanning electron microscope, there are often deep scratches on the surface of cleaned teeth, which are easy for plaque to adhere and The formation of calculus nuclei, which will lead to rapid growth of dental calculus, leading to peri...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): A61K8/24A61K8/02A61K8/19A61Q11/00
CPCY02P10/25
Inventor 宋雨来李高洁徐文洲
Owner JILIN UNIV