The invention discloses a synthetic method of 2,6 dihydroxy
naphthalene, which comprises the following steps: placing 2,6 dihydroxy
naphthalene in an alkali fusion pan, then a mixture of
solid sodium hydroxide and
nitrate is placed, Slowly heating to 150-170 DEG C, stirring, continuously heating to 320 DEG C, insulating for fusing alkali for 2.5-3.5 hours at 310-330 DEG C, then cooling to 200 DEG C, slowly dropping 450g of water for diluting, using a tri(octyl-decyl)amine solution for extracting 2,6-dihydroxy
naphthalene, then acidifying the extracted 2, 6-dihydroxy naphthalene by
sulfuric acid, and filtering and refining
filter cake by an
ethanol water mixed
solvent to obtain 2,6-dihydroxy naphthalene. According to the synthetic method of 2,6-dihydroxy naphthalene, the used
inorganic solvent is a mixture of
potassium nitrate,
sodium nitrite and
sodium nitrate. According to the invention,
viscosity of an alkali fusion material is low, fluidity is good, material can be uniformly mixed, and alkali fusion effect is good. In addition, under high temperature condition for alkali fusion, no
decomposition problem of oxidation
organic matter is generated, and no difficult separating problem is generated for the mixture.