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Ceramic coating member for semiconductor processing apparatus

A technology for processing devices and covering components, which is applied in semiconductor/solid-state device manufacturing, superimposed layer plating, electrical components, etc., can solve problems such as corrosive environments and instrument damage, and achieve improved plasma output, increased productivity, and improved The effect of etch effect and speed

Active Publication Date: 2012-05-30
TOKYO ELECTRON LTD +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Moreover, in the plasma environment of the F-containing gas atmosphere, since the above reaction is promoted, it becomes a very serious corrosive environment.
Moreover, corrosion product particles are generated in such an environment, and they fall and adhere to the surface of the integrated circuit of the semiconductor product, causing damage to the device

Method used

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  • Ceramic coating member for semiconductor processing apparatus
  • Ceramic coating member for semiconductor processing apparatus
  • Ceramic coating member for semiconductor processing apparatus

Examples

Experimental program
Comparison scheme
Effect test

experiment example 1

[0076] In this experimental example, the state of sputtered film formation of Group IIIB element oxides, and the state of the layer formed when electron beam irradiation and laser beam irradiation were performed on the obtained film were investigated. In addition, Sc 2 o 3 , Y 2 o 3 , La 2 o 3 , CeO 2 、Eu 2 o 3 、Dy 2 o 3 and Yb 2 o 3 Seven kinds of oxide powders (average particle size: 10-50 μm). Then, these powders are directly sprayed with a thickness of 100 μm by atmospheric plasma spraying (APS) and reduced pressure plasma spraying (LPPS) on one side of an aluminum test piece (size: width 50mm x length 60mm x thickness 8mm). coating. Then, the surfaces of these films were subjected to electron beam irradiation treatment and laser beam irradiation treatment. Table 1 summarizes the results of this experiment.

[0077] In addition, the actual results of the spraying of lanthanide metal oxides with atomic numbers from 57 to 71 have not been reported so far. Ther...

experiment example 2

[0085] In this experimental example, from the test piece after the high-energy irradiation treatment made in the above-mentioned test 1, for Y 2 o 3 For the sprayed coating, observe the section of the sprayed coating before and after the electron beam irradiation treatment with an optical microscope, and observe the changes in the microstructure of the film produced by the high-energy irradiation treatment.

[0086] figure 1 is schematically denoting Y 2 o 3 Changes in the microstructure near the surface of a thermally sprayed film (porous film), a film subjected to electron beam irradiation treatment, and a composite film with an undercoat layer. exist figure 1 In the non-irradiation-treated test piece shown in (a), it can be seen that the sprayed particles constituting the film exist independently, and the surface roughness is large. on the other hand, figure 1 (b) shows that a new layer having a different microstructure was formed on the above-mentioned sprayed coatin...

experiment example 3

[0089] This experimental example is determined by XRD figure 1 (a) Y 2 o 3 The porous layer of the sprayed film, and the porous layer produced by electron beam irradiation under the following conditions figure 1 The secondary recrystallized layer shown in (b) was studied for the crystal structure of each layer. figure 2 To show this result, an XRD pattern before electron beam irradiation treatment is shown. and, image 3 is an X-ray diffraction pattern on the vertical axis before the enlargement process. Figure 4 It is the X-ray diffraction pattern of the vertical axis after enlargement processing. Depend on image 3 It was found that in the sample before treatment, a peak indicating monoclinic crystals was observed particularly in the range of 30 to 35°, and it was found that cubic crystals and monoclinic crystals were in a mixed state. In contrast, as Figure 4 Shown, means Y 2 o 3 The peaks of the particles become sharper, the peaks of monoclinic crystals attenu...

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Abstract

A ceramic coating member is provided for improving durability of a member arranged inside a container of a semiconductor processing apparatus for performing plasma etching process or the like under strong corrosion resistant environment. A porous layer composed of a sprayed coating of an oxide material in the group IIIa in the periodic table is provided on the front plane of a metal or nonmetal base material, directly or through an undercoat layer. On the layer, a secondary recrystallized layer is formed by irradiation of high energy of electronic beams, laser beams and the like.

Description

technical field [0001] The present invention relates to a ceramic covering member for semiconductor processing equipment, and is particularly suitable as a covering member for members, parts, etc. arranged in a semiconductor processing container for performing plasma etching processing or the like. Background technique [0002] Equipment used in the field of semiconductors and liquid crystals is often processed using plasma energy of a highly corrosive halogen-based etching gas. For example, by semiconductor processing equipment, plasma is generated in a fluorine-based or chlorine-based corrosive gas atmosphere or a mixed gas atmosphere of these gases and an inert gas. Processing (etching) to form a fine wiring pattern. [0003] In the case of this processing technology, at least a part of the wall surface of the reaction vessel or the components or parts (pedestal, electrostatic chuck, electrode, etc.) arranged inside it are easily corroded by plasma energy. Therefore, It...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C23C4/10C23F4/00H01L21/02B32B5/00
CPCC23C4/18C23C28/042C23C4/02C23C4/105C23C26/00C23C4/11C23C28/00
Inventor 小林义之村上贵宏原田良夫竹内纯一山崎良小林启悟
Owner TOKYO ELECTRON LTD
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