Electro-deposition preparation method for Fe-Co soft magnetic film
A soft magnetic thin film and electrodeposition technology, applied in the application of magnetic film to substrate, magnetic layer, electrolytic inorganic material coating, etc., can solve the problems of harsh conditions, complicated operation, huge equipment cost, etc., and achieve mild and reliable reaction conditions control, high preparation efficiency and low cost
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Embodiment 1
[0041] Electrodeposition preparation of iron-cobalt alloy soft magnetic thin film:
[0042] 1. Carry out mechanical pretreatment on the deposition matrix material: rough grinding with sandpaper to remove burrs, oxide layers, etc. on the surface of the sample, and reduce the surface roughness;
[0043] 2. Pre-treatment of the copper substrate sample:
[0044] Alkaline cleaning and pickling are carried out sequentially on the copper substrate samples. The components of the alkaline cleaning solution for degreasing and rust removal of the substrate are: sodium hydroxide 35g / L, sodium dihydrogen phosphate 8g / L; the temperature of the alkaline cleaning for degreasing and rust removal is controlled at 50°C, and the time is controlled at 8 minutes;
[0045] The sample is electropolished, and the formula of the solute in the electropolishing solution is: citric acid 20g / L, ammonium citrate 46g / L;
[0046] The process parameters of the electrolytic polishing are as follows: the elect...
Embodiment 2
[0060] Electrodeposition preparation of iron-cobalt alloy soft magnetic thin film:
[0061] 1. Carry out mechanical pretreatment on the deposition matrix material: rough grinding with sandpaper to remove burrs, oxide layers, etc. on the surface of the sample, and reduce the surface roughness;
[0062] 2. Pretreatment of the sample copper sheet:
[0063] Alkaline cleaning and acid cleaning are performed on the samples in turn. The components of the alkaline cleaning solution for degreasing and rust removal of the substrate are: sodium hydroxide 35g / L, sodium dihydrogen phosphate 8g / L; the temperature of the alkaline cleaning for degreasing and rust removal is controlled at 50°C, and the time is controlled at 8 minutes;
[0064] The sample is electropolished, and the formula of the solute in the electropolishing solution is: citric acid 20g / L, ammonium citrate 46g / L;
[0065] The process parameters of the electrolytic polishing are as follows: the electrolytic polishing anode ...
Embodiment 3
[0078] Electrodeposition preparation of iron-cobalt alloy soft magnetic thin film:
[0079] 1. Carry out mechanical pretreatment on the deposition matrix material: rough grinding with sandpaper to remove burrs, oxide layers, etc. on the surface of the sample, and reduce the surface roughness;
[0080] 2. Pretreatment of the sample copper sheet:
[0081] The samples were sequentially washed with alkali and acid. The components of the alkaline cleaning solution for degreasing and rust removal of the substrate are: sodium hydroxide 35g / L, sodium dihydrogen phosphate 8g / L; the temperature of the alkaline cleaning for degreasing and rust removal is controlled at 50°C, and the time is controlled at 8 minutes;
[0082] The sample is electropolished, and the formula of the solute in the electropolishing solution is: citric acid 20g / L, ammonium citrate 46g / L;
[0083] The process parameters of the electrolytic polishing are as follows: the electrolytic polishing anode is a copper she...
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