Method for utilizing ink-jet printing technology to prepare photonic crystal composite membrane with responsiveness and patterning

A technology of inkjet printing and photonic crystals, which is applied in the direction of copying/marking methods, household utensils, printing, etc., can solve the problems of widening photonic crystals, achieve low cost, simple process, and increase the speed of absorbing and releasing responsive substances.

Inactive Publication Date: 2013-06-19
INST OF CHEM CHINESE ACAD OF SCI +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, the photonic crystal composite film with ultrafast response and patterning obtained by inkjet printing has not been reported yet. The simple and rapid preparation of photonic crystal

Method used

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  • Method for utilizing ink-jet printing technology to prepare photonic crystal composite membrane with responsiveness and patterning
  • Method for utilizing ink-jet printing technology to prepare photonic crystal composite membrane with responsiveness and patterning
  • Method for utilizing ink-jet printing technology to prepare photonic crystal composite membrane with responsiveness and patterning

Examples

Experimental program
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Effect test

Embodiment 1

[0054] At a temperature of 10°C and a humidity of 20%, the monodisperse poly(styrene-methyl methacrylate-acrylic acid) triblock copolymer with a particle size of 100nm prepared by the method of patent No. ZL200510011219.2 Emulsion of latex particles, responsive functional monomer acrylamide, crosslinking agent N, N-methylenebisacrylamide, photoinitiator 2-hydroxy-2-methyl-1-phenyl-1-propanone, high The boiling point additive ethylene glycol and water are mixed to obtain a mixed solution, wherein the content of the monodisperse poly(styrene-methyl methacrylate-acrylic acid) triblock copolymer latex particles in the mixed solution is 20wt%, and the responsive function unit The content of bulk acrylamide is 20wt%, the content of crosslinking agent N, N-methylenebisacrylamide is 5wt%, the content of photoinitiator 2-hydroxyl-2-methyl-1-phenyl-1-acetone 5wt%, the content of high-boiling additive ethylene glycol is 20wt%, and the balance is water; the above-mentioned mixed solution ...

Embodiment 2

[0058] At a temperature of 40°C and a humidity of 60%, commercially available monodisperse polymethyl methacrylate latex particles with a particle size of 1100 nm, responsive functional monomer acrylamide, and cross-linking agent N, N-methylene Bisacrylamide, thermal initiator water-soluble ammonium persulfate, high boiling point additive ethylene glycol and water are mixed to obtain a mixed solution, wherein the content of monodisperse polymethyl methacrylate latex particles in the mixed solution is 5wt%, and the response The content of the functional monomer acrylamide is 1wt%, the content of the crosslinking agent N, N-methylenebisacrylamide is 0.1wt%, the content of the thermal initiator water-soluble ammonium persulfate is 0.1wt%, the high boiling point The content of the auxiliary agent ethylene glycol is 30wt%, and the balance is water; the above-mentioned mixed solution is installed in the ink cartridge of an inkjet printer with a nozzle aperture of 100 μm, and the poly...

Embodiment 3

[0062]At a temperature of 20°C and a humidity of 40%, the monodisperse poly(styrene-methyl methacrylate-acrylic acid) triblock copolymer with a particle size of 180nm prepared by the method of patent No. ZL200510011219.2 Emulsion of latex particles, responsive functional monomer acrylamide, crosslinking agent N, N-methylenebisacrylamide, photoinitiator 2-hydroxy-2-methyl-1-phenyl-1-propanone, high The boiling point additive ethylene glycol and water are mixed to obtain a mixed solution, wherein the content of the monodisperse poly(styrene-methyl methacrylate-acrylic acid) triblock copolymer in the mixed solution is 20wt%, and the responsive functional monomer propylene The content of amide is 15wt%, crosslinking agent N, the content of N-methylenebisacrylamide is 2.5wt%, the content of photoinitiator 2-hydroxyl-2-methyl-1-phenyl-1-acetone is 2.5wt%, the content of high-boiling additive ethylene glycol is 40wt%, and the balance is water; the above-mentioned mixed solution is in...

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Abstract

The invention relates to a method for utilizing an ink-jet printing technology to simply and quickly prepare a photonic crystal composite membrane with ultrafast responsiveness and patterning. The method for utilizing the ink-jet printing technology to prepare the photonic crystal composite membrane with responsiveness and patterning utilizes mixed liquor of monodisperse emusion particles, a monomer of a responsiveness function polymer, a cross-linking agent, an initiator, a high boiling point addictive and water as ink, the ink-jet printing technology is used for acquiring the photonic crystal composite membrane which is a patterning composed of microdroplet units, and the photonic crystal composite membrane is in response to humidity, to temperature, to acid gas, and/or to alkaline gas. The microdroplet units are piled up by frameworks of the monodisperse emulsion particles, and a responsiveness cross-linking polymer acquired by the monomer of the responsiveness function polymer through cross-linking polymerization is filled in gaps of the frameworks of the monodisperse emulsion particles. The photonic crystal composite membrane can not only achieve visual detection by distinguishing color change through naked eyes of people, but also have wide application prospect in quick intelligent display unit caused by external environment change, dangerous substance detection, chemical reaction monitoring, photoswitch, integrated optical circuit, and the like.

Description

technical field [0001] The invention belongs to the technical field of preparation of colloidal photonic crystal films, and in particular relates to a method for simply and rapidly preparing a photonic crystal composite film with ultrafast response and patterning by using inkjet printing technology. Background technique [0002] Since the concept of photonic crystals was proposed in 1987, after more than 20 years of development, it has become a research hotspot of common concern in the fields of physics, optoelectronics, materials science, chemistry, and nanotechnology. Based on the various special properties of known photonic crystals, its applications cover many fields such as light, electricity, catalysis, sensing, display, and detection. In the usual patent literature, colloidal photonic crystal films are mainly used in filters (such as CN: 01105105.1, CN: 98110990.X), optical switches (CN: 02160207.7), optical waveguides (CN: 02804125.9, CN: 99810798, CN: 01132293.4, C...

Claims

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Application Information

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IPC IPC(8): B41M5/00B41J2/01C09D11/10C09D11/40
Inventor 王利彬王京霞周金明宋延林
Owner INST OF CHEM CHINESE ACAD OF SCI
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