Copolyester melt direct-spinning controllable multiple differential shrinkage composite fiber and preparation method thereof
A melt direct spinning and composite fiber technology, applied in the field of chemical fiber, can solve the problems of poor composite uniformity of polyester differential shrinkage composite fiber, poor dyeing rate of polyester fiber fabric, poor moisture absorption, breathability and moisture retention, etc., achieving cost performance Obvious advantages, good fluffiness, moisture absorption, breathability and good moisturizing effect
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Embodiment 1
[0024] This example provides a method for preparing controllable multi-shrinkage composite fibers by direct spinning of copolyester melt of 155dtex / 192f (where the specification of fully drawn yarn is 108dtex / 144f, and the specification of pre-oriented yarn is 47dtex / 48f). Its production process conditions are as follows:
[0025] Inject the mixture of 70% terephthalic acid (PTA) and 30% ethylene glycol (EG) into the slurry tank, add catalyst ethylene glycol antimony 0.04% and additives trimethyl phosphate 0.01%, acetic acid Cobalt 0.011%, sodium acetate 0.005%, mixed and stirred, pumped into the first esterification tank through the slurry crank pump for esterification reaction, and then automatically flowed into the second esterification tank through the liquid level difference, and at the same time added a mass fraction of 1.0 %The third component polyethylene glycol and 0.007% mass fraction of the fourth component diethylene glycol and 0.01% mass fraction of the fifth comp...
Embodiment 2
[0037] This example provides a method for preparing controllable multi-shrinkage composite fibers by direct spinning of 138dtex / 108f (including: fully drawn yarn specification 55dtex / 36f, pre-oriented yarn specification 83dtex / 72f) copolyester melt. According to the technology of Example 1, the production process and conditions of this example are as follows: inject the mixed ingredients with mass fraction of 70% terephthalic acid (PTA) and mass fraction of 30% ethylene glycol (EG) into the slurry tank, add The catalyst ethylene glycol antimony 0.04% and the additives trimethyl phosphate 0.01%, cobalt acetate 0.011%, sodium acetate 0.005%, mixed and stirred, pumped into the first esterification tank through the slurry crank pump to carry out the esterification reaction, and then passed the liquid Potential difference automatically flows into the second esterification tank, and at the same time add the third component polyethylene glycol with a mass fraction of 1.0%, the fourth ...
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