Calcium-doped inorganic nanocomposite material for 3D printing and preparation method of calcium-doped inorganic nanocomposite material

An inorganic nano-composite material technology, applied in the field of 3D printing manufacturing, can solve the problems of high price, restrict the promotion and popularization of 3D printing technology, etc., achieve a wide range of acquisition, good compounding effect, and improve the effect of density and strength

Inactive Publication Date: 2015-03-25
QINGDAO MATE RUIOU NEW MATERIAL TECH CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

At present, the 3D printing molding materials sold in the market are basically monopolized by foreign companies, and the price is high, which seriously restricts the promotion and popularization of 3D printing technology in my country.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0029] A calcium-doped inorganic nanocomposite material for 3D printing, comprising: 73% aluminum oxide, 6% nano-zinc oxide, 2% calcium powder, 4% polyethylene glycol, 10% Silica sol, 1% sodium silicate solution added with silicon oxide, titanium oxide and aluminum oxide, 4% ethanol; the particle size of nano-zinc oxide is 40 nanometers; the solid phase volume fraction of silica sol is 40%; The mass ratio of silicon oxide, titanium oxide, aluminum oxide and sodium silicate in the sodium silicate solution is 2:1:1:4.

[0030] The preparation method of this calcium-doped inorganic nanocomposite material is:

[0031] (1) the polyethylene glycol that accounts for gross weight 4% is dissolved in the ethanol that accounts for gross weight 2%, and the tensio-active agent solution that forms concentration is 8g / L, will account for the nano zinc oxide of gross weight 6%. In the surfactant solution, ultrasonically stir for 30 minutes to form a suspension of the modified nano-powder rei...

Embodiment 2

[0035] A calcium-doped inorganic nanocomposite material for 3D printing, comprising: 75% aluminum nitride, 8% nano-zinc oxide, 3% calcium powder, 5% polyvinyl alcohol, 5% Silica sol, 1% sodium silicate solution added with silicon oxide, titanium oxide and aluminum oxide, 3% acetone; the particle size of nano-zinc oxide is 20 nanometers; the solid phase volume fraction of silica sol is 10%; silicic acid The mass ratio of silicon oxide, titanium oxide, aluminum oxide and sodium silicate in the sodium solution is 2:1:1:4.

[0036] The preparation method of this calcium-doped inorganic nanocomposite material is:

[0037] (1) dissolving polyethylene glycol accounting for 5% of the total weight in the acetone accounting for 1% of the total weight, and forming a concentration of 10g / L surfactant solution, will account for 8% of the total weight of nano-zinc oxide added to the In the surfactant solution, ultrasonically stir for 60 minutes to form a suspension of the modified nano-pow...

Embodiment 3

[0041] A calcium-doped inorganic nanocomposite material for 3D printing, in terms of weight percentage, comprising: 78% silicon oxide, 5% nano-titanium oxide, 2% calcium powder, 3% tributyl phosphate, 8% Silica sol, 1% sodium silicate solution added with silicon oxide, titanium oxide and aluminum oxide, 3% methanol; the particle size of nano-titanium oxide is 60 nanometers; the solid phase volume fraction of silica sol is 20%; silicon The mass ratio of silicon oxide, titanium oxide, aluminum oxide and sodium silicate in the sodium silicate solution is 2:1:1:4.

[0042] The preparation method of this calcium-doped inorganic nanocomposite material is:

[0043](1) Dissolve the tributyl phosphate accounting for 3% of the total weight in the methanol of 1% of the total weight, and form a concentration of 6g / L surfactant solution, add 5% of the total weight of nano-titanium oxide to the In the surfactant solution, ultrasonically stir for 50 minutes to form a suspension of the modif...

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Abstract

The invention discloses a calcium-doped inorganic nanocomposite material for 3D printing. The calcium-doped inorganic nanocomposite material comprises the following components in percentage by weight: 73-80% of ceramic precursor powder, 5-10% of nano-powder reinforcing material, 2-5% of calcium powder, 2-5% of a surfactant, 2-5% of an organic solvent, 1-4% of an inorganic binder and 5-10% of a low-temperature curing agent, wherein the particle size of the nano-powder reinforcing material is 20-200nm. By adopting the surfactant to perform deaggregation treatment on nano-powder, the nano-powder has excellent dispersivity; by adding the nano-powder into the ceramic precursor powder, the density and strength of ceramic can be improved, and the toughness of a product can be further upgraded; by mutually coordinating and matching the inorganic mixed powder, the inorganic binder and the low-temperature curing agent, the fast binding can be realized at low temperature; and the inorganic nanocomposite material can be used as a molding raw material of a 3D printing fast molding machine, the fast molding on the 3D printing machine can be effectively realized, and the calcium-doped inorganic nanocomposite material can be applied to a variety of types of 3D printing machines.

Description

technical field [0001] The invention relates to the technical field of 3D printing manufacturing, in particular to a calcium-doped inorganic nanocomposite material for 3D printing and a preparation method thereof. technical background [0002] Rapid prototyping technology was born in the late 1980s. It is a high-tech manufacturing technology based on material accumulation method. It is considered to be a major achievement in the manufacturing field in recent years. It integrates mechanical engineering, CAD, reverse engineering technology, layered manufacturing technology, numerical control technology, material science, and laser technology, and can automatically, directly, quickly and accurately transform design ideas into prototypes with certain functions or directly manufacture parts , so as to provide a high-efficiency and low-cost realization means for parts prototype production and verification of new design ideas. That is, rapid prototyping technology is to use the da...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C04B35/10C04B35/581C04B35/582C04B35/14C04B35/584C04B35/565C04B35/626
Inventor 岑伟郭雷
Owner QINGDAO MATE RUIOU NEW MATERIAL TECH CO LTD
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