Aluminium-oxide-based spark plug insulation material and preparation method thereof
A technology based on spark plugs and insulating materials, applied in the field of alumina-based spark plug insulating materials and their preparation, can solve the problems of insulator breakdown and the like
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[0029] The embodiment of the present invention discloses a preparation method of an alumina-based spark plug insulating material, which includes the following steps:
[0030] 95-97 parts by weight of alumina powder, 1-3 parts by weight of silicon dioxide powder, 0.5-1 part by weight of magnesium carbonate powder, 0.2-0.5 parts by weight of calcium carbonate powder, 0.2-0.5 parts by weight of barium carbonate powder, lanthanum oxide powder 0.1 to 0.5 parts by weight, 0.2 to 0.5 parts by weight of yttrium oxide powder, 0.1 to 0.5 parts by weight of scandium oxide powder and 0.1 to 0.3 parts by weight of titanium oxide powder are added to the ball mill, mixed and pulverized by alumina balls, and the ball milling time is 10~ 14h, obtain the first mixed material;
[0031] The first mixed material is heated to 300°C under a mixed atmosphere of nitrogen and oxygen, and the second mixed material is obtained after gravity-free mixing;
[0032] The second mixed material is filtered and...
Embodiment 1
[0048] The raw material powder feeding ratio of firing the alumina-based sintered body is: 95.5 parts by weight of alumina powder, 2 parts by weight of silicon dioxide powder, 0.5 part by weight of magnesium carbonate powder, 0.4 part by weight of calcium carbonate powder, and 0.4 part by weight of barium carbonate powder, 0.25 parts by weight of lanthanum oxide powder, 0.5 parts by weight of yttrium oxide powder, 0.25 parts by weight of scandium oxide, and 0.2 parts by weight of titanium oxide powder.
[0049] Put the above raw material powder into the QM-3B high-speed vibrating ball mill, and use alumina balls with a diameter of 10mm for mixing and crushing. The ball milling time is 10h, and the material is discharged after the ball milling is completed.
[0050] Add raw material powder after ball milling figure 1 In the shown improved heatable atmosphere control gravity-free mixer (volume 3L), the control intake composition is nitrogen: oxygen=9:1 (volume ratio), the contro...
Embodiment 2
[0054] The raw material powder feeding ratio of firing the alumina-based sintered body is: 96 parts by weight of alumina powder, 2 parts by weight of silicon dioxide powder, 0.5 part by weight of magnesium carbonate powder, 0.5 part by weight of calcium carbonate powder, 0.2 part by weight of barium carbonate powder, 0.25 parts by weight of lanthanum oxide powder, 0.5 parts by weight of yttrium oxide powder, 0.25 parts by weight of scandium oxide, and 0.1 part by weight of titanium oxide powder.
[0055] Put the above raw material powder into the QM-3B high-speed vibrating ball mill, and use alumina balls with a diameter of 10mm for mixing and crushing. The ball milling time is 10h, and the material is discharged after the ball milling is completed.
[0056] The raw material powder after ball milling is added as figure 1 In the shown improved heatable atmosphere control gravity-free mixer (volume 3L), the intake composition is controlled to be nitrogen: oxygen = 9:1 (volume ra...
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