Efficient cyfluthrin aqueous-dispersion nano composite granule and preparation method thereof

A high-efficiency cyfluthrin, nano-composite technology, applied in the fields of botanical equipment and methods, pesticides, biocides, etc., can solve the problems of large pesticide residues, microbial decomposition, no controlled release effect, etc., to reduce pesticide costs, optimize Microstructure, effect of significant technical advantages

Inactive Publication Date: 2015-05-27
WUHAN UNIV OF TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] (1) Contains a large amount of organic solvents such as toluene and xylene, causing great environmental pollution;
[0004] (2) No controlled release effect and poor adhesion to the target, resulting in low bioavailability and short validity period of the pesticide;
[0005] (3) It is easy to be decomposed by light and microorganisms, resulting in a decrease in drug efficacy;
[0006] (4) When used, it needs to be diluted with water to form an emulsion. The active ingredients are micron-scale dispersed, with poor dispersibility and low effective utilization rate, resulting in a large amount of pesticides, resulting in increased costs, large pesticide residues, and seriously affecting the quality of agricultural products.

Method used

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  • Efficient cyfluthrin aqueous-dispersion nano composite granule and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0036] Beta-cyfluthrin water-dispersible nanocomposite granules are prepared by the following method: Accurately weigh 20.0 kg of beta-cyfluthrin loaded on nano-titanium dioxide according to the formula requirements, and the wetting agent is 1.0 kg of alkylnaphthalene sulfonic acid condensation polymer TERSPERSE2425, and disperse The agent is 10.0kg of polycarboxylate TERSPERSE2700, the disintegrating agent is 1.0kg of urea, the filler is 67.9kg of white carbon black, add 15-20kg of water and mix it evenly to obtain a water suspension system, and then use ultra-fine wet Grind to a fineness of 100-600nm, add a certain amount of water and 0.1kg of binder to obtain a slurry for spraying, and then send the slurry to a drying tower for spray drying at 140°C for granulation. The residual moisture content of the final product is 0.5-1.0 wt%, and finally the materials are jointly screened by a vibrating fluidized bed and a vibrating sieve to obtain water-dispersed nanocomposite granule...

Embodiment 2

[0039]Beta-cyfluthrin water-dispersible nanocomposite granules are prepared by the following method: accurately weigh 41.2 kg of beta-cyfluthrin loaded on nano-silica according to the formula requirements, and the wetting agent is 2.0 kg of sodium lauryl sulfate, and disperse The agent is 5.0kg of polycarboxylate TERSPERSE2700, the disintegrant is 2.0kg of magnesium sulfate, 3.0kg of ammonium sulfate, the filler is 20.0kg of bentonite, 23.8kg of kaolin, add 15-20kg of water and mix them evenly , to obtain a water suspension system, and then use an ultra-fine wet grinder to grind to a fineness of 100-600nm, add a certain amount of water and 3.0kg of stabilizer to obtain a slurry for spraying, and then send the slurry to a drying tower, Spray drying and granulation at 130°C. After granulation, the residual moisture content of the product is 0.5-1.0wt%. Finally, the material is screened jointly by a vibrating fluidized bed and a vibrating sieve to obtain water-dispersed nano-parti...

Embodiment 3

[0042] Beta-cyfluthrin water-dispersible nanocomposite granules are prepared by the following method: accurately weigh 50.0 kg of beta-cyfluthrin loaded on nano-copper hydroxide according to the formula requirements, and the wetting agent is 3.0 kg of Morwet EFW, 3.0 kg of Twelve Sodium alkylbenzenesulfonate, polycarboxylate TERSPERSE2700 of 3.0kg as dispersant, TERSPERSE2425 of alkylnaphthalenesulfonic acid condensation polymer of 4.0kg, magnesium sulfate of 5.0kg as disintegrant, 5.0kg of soluble starch, filler bentonite 11.5 kg, 10.5kg of white carbon black, add 15-20kg of water and mix it evenly to obtain a water suspension system, then use an ultra-fine wet grinder to grind to a fineness of 100-600nm, add a certain amount of water and 5.0kg of Effect agent to obtain the slurry for spraying, then send the slurry to the drying tower, spray dry and granulate at 160°C, the residual moisture content of the product after granulation is 0.5-1.0wt%, and finally the material is vib...

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Abstract

The invention discloses an efficient cyfluthrin aqueous-dispersion nano composite granule and a preparation method thereof. The efficient cyfluthrin aqueous-dispersion nano composite granule is prepared from the following raw materials in percentage by weight: 20-80% of efficient cyfluthrin loaded on a nano carrier, 1.0-10.0% of a wetting agent, 2.0-10.0% of a dispersing agent, 1.0-10.0% of a disintegrating agent, 0.1-5% of other auxiliaries, and the balance of a filler. The preparation method of the efficient cyfluthrin aqueous-dispersion nano composite granule adopts a wet-process process to prepare a disintegrating and dispersing type aqueous-dispersion granule through an equal-grain-size spraying and pelletizing technology. Compared with a conventional granule, the efficient cyfluthrin aqueous-dispersion nano composite granule has the unique advantages of being long-acting in slow release, low in loss rate and residues, small in toxicity, high in safety, good in environmental compatibility and the like, can be widely applied to various insect pests in a farmland, an orchard and a vegetable field, and has an important application value.

Description

technical field [0001] The invention belongs to the field of pesticide preparations, in particular to a water-dispersed nanocomposite granule of beta-cyfluthrin and a preparation method thereof. Background technique [0002] Beta-cyfluthrin is the product of epimerization of cyfluthrin, also known as Bastree. In addition to the insecticidal spectrum and characteristics of ordinary cyfluthrin, the biggest advantage of this product is that it has higher insecticidal activity. The insecticidal activity is Twice that of ordinary cyfluthrin, the recommended dosage is only 0.4-1.3g (active ingredient) / mu. Cyfluthrin has strong contact and stomach poisoning effects, slight penetration but no systemic effect, broad insecticidal spectrum, and long-lasting effect. It can effectively control the pests of Coleoptera, Hemiptera, Homoptera and Lepidoptera on grain and oil crops (such as corn, wheat, peanut, soybean, etc.) and economic crops (if trees, tobacco and vegetables, etc.), such ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): A01N53/08A01N25/14A01P7/04
Inventor 夏涛任红轩刘扬石晓敏黄进原弘
Owner WUHAN UNIV OF TECH
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