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Glass bead used for highway-engineering-grade light reflection film and preparation method for glass bead

A glass microbead, engineering-grade technology, applied in the field of glass microbeads and its preparation, can solve problems such as unstable quality and performance, improve mechanical strength and optical performance, long service life, improve aging resistance and high temperature resistance sexual effect

Inactive Publication Date: 2015-09-23
HEFEI DINGLIANG OPTICAL TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

At present, the quality and performance of glass microsphere products produced by Chinese manufacturers are unstable, and there is still a certain gap compared with foreign glass microsphere products.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment Construction

[0015] A glass microsphere used for highway engineering grade reflective film, made of the following raw materials by weight (kg): Dickite 48, Cancryptite 36, Magnesium Carbonate 14, Calcite 32, Silica Powder 59, Kyanite 23 , calcium tetrafluoroborate 8, antimony trioxide 9, coke powder 7, lithium niobate 6, potassium chloride 7, additive 11;

[0016] The additive is mixed from the following raw materials by weight (kg): Bismuth oxychloride 8, cerium phosphate 10, cobalt chromate 7, barium peroxide 4.5, sodium selenate 5.5, indium tin oxide 3, yttrium oxalate 5, disilicide Molybdenum 9, strontium titanate 6.

[0017] A preparation method for glass microspheres used in highway engineering grade reflective film, comprising the following steps:

[0018] (1) Mix dickite, cancryptite, calcite and kyanite evenly, calcinate at 690-760°C for 1.5-2h, air-cool to room temperature, crush, pass through 80-120 mesh sieve, add 7-9 times the amount of water , 2000-3000r / min we...

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PUM

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Abstract

The invention discloses a glass bead used for a highway-engineering-grade light reflection film and a preparation method for the glass bead. The glass bead is prepared from the following raw materials in parts by weight: 36-54 parts of dickite, 28-42 parts of cancrinite, 12-18 parts of magnesium carbonate, 22-36 parts of calcite, 44-68 parts of silica powder, 18-29 parts of kyanite, 6-12 parts of calcium tetrafluoroborate, 7-13 parts of antimonous oxide, 5-10 parts of coke powder,4-9 parts of lithium niobate, 5-10 parts of potassium chloride and 9-14 parts of additives. According to the glass bead, the lithium niobate, the calcium tetrafluoroborate, the calcite, the dickite, the cancrinite, the kyanite and the silica powder have synergistic effect, and the raw materials act with one another, so that not only can the ageing resistance and the high temperature resistance of the glass bead be improved, but also the mechanical strength and the optical performance of the glass bead can be improved. The glass bead prepared by the preparation method disclosed by the invention has the advantages such as high strength, high brightness of reflected light, high temperature resistance, ageing resistance and the like, is long in service life, safe and reliable, and can be widely applied to the highway-engineering-grade light reflection film.

Description

technical field [0001] The invention relates to a glass microsphere used for road engineering grade reflective film and a preparation method thereof, belonging to the field of glass microsphere manufacture. Background technique [0002] Glass beads refer to solid or hollow glass beads with a diameter of several microns to hundreds of microns, which are divided into two types: colorless and colored. Those with a diameter of 0.8mm or more are called fine beads; those with a diameter of less than 0.8mm are called microbeads. Glass beads are a new type of silicate material, which are widely used because of their characteristics of transparency, adjustable refractive index, directional retroreflection, smooth surface, good fluidity, electrical insulation, stable chemical properties, heat resistance and high mechanical strength. Applied to reflective film. [0003] The reflective film is based on the principle of retro-reflective glass beads with high refractive index. It can r...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C03C12/02C03C6/06
Inventor 范春平
Owner HEFEI DINGLIANG OPTICAL TECH