Green and environment-friendly method for preparing alkaline water-soluble chitosan derivative
A green environmental protection, water-soluble shell technology, applied in the field of preparing alkaline water-soluble chitosan derivatives, can solve the problems of heavy pollution, large consumption of reagents, not in line with the concept of green environmental protection, etc., and achieves mild reaction conditions, good water solubility, The effect of high molecular weight
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Embodiment 1
[0037] A preparation method of chitosan water-soluble derivatives, comprising the following steps: 1) preparation of chitosan grafted polyacrylic acid
[0038] Using water as a solvent, put it in an oil bath at 60 ° C, and after purging the air with nitrogen, according to the mass ratio of chitosan and acrylic acid monomer is 1:6 (w / w), acrylic acid is passed through constant pressure drop Slowly add the funnel dropwise into the aqueous solution mixing system of reactive chitosan, after fully mixing, slowly add 3.28×10 -3 mol / L cerium ammonium nitrate (Ce 4+ ) as an initiator, after the dropwise addition, continue to deoxidize with nitrogen, maintain the original temperature at 60° C. for 5 h, and stop the reaction. Precipitate with concentrated hydrochloric acid, then filter the solution, wash the solid with 99% ethanol for three times, and then filter under reduced pressure to remove the homopolymer of acrylic acid. After vacuum drying at 50°C, a solid chitosan grafted poly...
Embodiment 2
[0046] A preparation method of chitosan water-soluble derivatives, comprising the following steps:
[0047] 1) Preparation of chitosan grafted polyacrylamide
[0048] Use water as a solvent, put it in an oil bath at 50°C, and after purging the air with nitrogen, pass acrylamide through constant pressure according to the mass ratio of chitosan and acrylamide monomer at a ratio of 1:10 (w / w). The dropping funnel was slowly added dropwise into the aqueous solution mixing system of the reaction chitosan, and after being fully mixed, slowly added 6×10 -3 mol / L cerium ammonium nitrate (Ce 4+ ) as an initiator, after the dropwise addition, continue to deoxidize with nitrogen, maintain the original temperature of 50° C. for 5 hours, and stop the reaction. Precipitate with concentrated hydrochloric acid, then filter the solution, wash the solid with 99% ethanol three times, and then filter under reduced pressure to remove the acrylamide homopolymer. After vacuum drying at 50°C, a sol...
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