A kind of mineral waste refractory material and its preparation process
A refractory material and a preparation process technology, applied in the field of refractory materials, can solve the problems of reducing the service life of refractory materials, poor mechanical toughness, increasing the damage rate of refractory products, etc., achieving easy large-scale production, simple preparation method, and solving environmental pollution. and waste of resources
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Embodiment 1
[0030] A mineral waste refractory material is prepared from the following raw materials in parts by weight: 50 parts of coal gangue, 120 parts of red mud, 10 parts of magnesium oxide, 4 parts of manganese oxide, 5 parts of titanium oxide, 2 parts of niobium pentoxide, and 15 parts of tough fiber; coal gangue is high-silicon coal gangue with a silicon oxide content of 48wt% and an alumina content of 13wt%; red mud is high-alumina red mud with an alumina content of 26wt% and a silica content of 12wt% , the calcium oxide content is 25wt%;
[0031] Wherein, the toughening fiber is a modified zirconia fiber, which is obtained through the following steps: 50 parts by weight of zirconia, after adding 3 parts by weight of calcium oxide and 1 part by weight of sodium oxide, and 400 parts by molar ratio of 1:1 The sodium chloride and potassium chloride compound salts were mixed and ground for 12 hours with absolute ethanol as the grinding medium, dried and calcined at 850°C for 6 hours,...
Embodiment 2
[0038]A mineral waste refractory material is prepared from the following raw materials in parts by weight: 50 parts of coal gangue, 130 parts of red mud, 13 parts of magnesium oxide, 5 parts of manganese oxide, 5.5 parts of titanium oxide, 3 parts of niobium pentoxide, and 17 parts of tough fiber; coal gangue is high-silicon coal gangue with a silicon oxide content of 49wt% and an alumina content of 14wt%; red mud is high-alumina red mud with an alumina content of 27wt% and a silica content of 13wt% , the calcium oxide content is 26wt%;
[0039] Wherein, the toughening fiber is a modified zirconia fiber, which is obtained through the following steps: 50 parts by weight of zirconia, after adding 3 parts by weight of calcium oxide and 1 part by weight of sodium oxide, and 400 parts by molar ratio of 1:1 The sodium chloride and potassium chloride compound salts were mixed and ground for 12 hours with absolute ethanol as the grinding medium, dried and calcined at 850°C for 6 hours...
Embodiment 3
[0046] A mineral waste refractory material is prepared from the following raw materials in parts by weight: 50 parts of coal gangue, 140 parts of red mud, 15 parts of magnesium oxide, 6 parts of manganese oxide, 6 parts of titanium oxide, 4 parts of niobium pentoxide, and 20 parts of tough fiber; coal gangue is high-silicon coal gangue with a silicon oxide content of 50wt% and an alumina content of 15wt%; red mud is high-alumina red mud with an alumina content of 28wt% and a silica content of 14wt% , the calcium oxide content is 27wt%;
[0047] Wherein, the toughening fiber is a modified zirconia fiber, which is obtained through the following steps: 50 parts by weight of zirconia, after adding 3 parts by weight of calcium oxide and 1 part by weight of sodium oxide, and 400 parts by molar ratio of 1:1 The sodium chloride and potassium chloride compound salts were mixed and ground for 12 hours with absolute ethanol as the grinding medium, dried and calcined at 850°C for 6 hours,...
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