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Preparation method of rice husk oligosaccharide

A technology of rice husk oligosaccharides and rice husks, which is applied in the field of preparation of rice husk oligosaccharides, can solve the problems of high water consumption in the treatment process, low yield of oligosaccharides, and difficult wastewater treatment, and achieve low cost and high water consumption , the effect of promoting rapid growth and reproduction

Inactive Publication Date: 2017-11-24
合肥市晶谷米业有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

This kind of sugar enters the large intestine as the proliferation factor of bifidobacteria, which can effectively promote the growth and reproduction of beneficial bacteria in the human body—bifidobacteria, and inhibit the growth of spoilage bacteria. Long-term consumption can slow down aging, laxative, antibacterial, cancer prevention, Anti-cancer, reduce the burden on the liver, and improve the rate of nutrient absorption, so oligosaccharides are a new generation of "future-type" functional food for the 21st century. It is a new product with a wide range of applications and application prospects. Popular, the development and application of oligosaccharides in my country started in the mid-1990s, and has developed rapidly in recent years. Rice husk is one of the main agricultural and sideline products in my country. The cost of making oligosaccharides from rice husks is low, so it is popular among oligosaccharide developers Welcome, at present, if cellulase is directly used to enzymatically hydrolyze rice husks, the enzymatic hydrolysis effect is poor, and the yield of oligosaccharides is extremely low. Rice husk fiber, and then use cellulase to enzymatically hydrolyze the fiber. Although this treatment process improves the yield of oligosaccharides, the treatment process consumes a lot of water, and the waste water generated is not easy to treat

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0020] Embodiment 1, a kind of preparation method of rice husk oligosaccharide, the steps are as follows:

[0021] (1) Crush the rice husk to 70 mesh, and treat it for 8 hours in an environment with a temperature of 0°C and a pressure of 1800 bar;

[0022] (2) After the treated rice husk is fully steamed and sterilized in steam, it is dried until the water content is 70%, and after cooling down to normal temperature, 10 parts of glucose, 0.01 part of ferrous sulfate, 0.02 part of thiamine, 0.01 part of riboflavin, 0.01 part of nicotinic acid, 0.01 part of dopamine hydrochloride, 0.01 part of sodium iodide and mix well;

[0023] (3) Inoculate cellulase into the rice husk, the inoculation ratio is 3‰, enzymatic hydrolysis at 35°C, and the enzymatic hydrolysis time is 38 hours;

[0024] (4) Mix the rice husk obtained by enzymatic hydrolysis with 3 times the volume of water evenly, introduce it into a high-speed centrifuge, and heat the surface of the centrifuge at the same time,...

Embodiment 2

[0027] Embodiment 2, a kind of preparation method of rice husk oligosaccharide, the steps are as follows:

[0028] (1) Crush the rice husk to 75 mesh, and treat it for 9 hours in an environment with a temperature of -1°C and a pressure of 1900 bar;

[0029] (2) After the treated rice husk is fully steamed and sterilized in steam, it is dried to a water content of 71%, and after cooling down to normal temperature, 11 parts of glucose, 0.012 parts of ferrous sulfate, 0.021 parts of thiamine, 0.011 parts of riboflavin, 0.012 parts of nicotinic acid, 0.0102 parts of dopamine hydrochloride, 0.0102 parts of sodium iodide and mix well;

[0030] (3) Cellulase was inoculated into the rice husk, the inoculation ratio was 4‰, enzymolysis was carried out at 36°C, and the enzymolysis time was 39 hours;

[0031] (4) Mix the rice husk obtained by enzymatic hydrolysis with 4 times the volume of water evenly, introduce it into a high-speed centrifuge, and heat the surface of the centrifuge at...

Embodiment 3

[0034] Embodiment 3, a kind of preparation method of rice husk oligosaccharide, the steps are as follows:

[0035] (1) Crush the rice husk to 80 mesh, and treat it for 10 hours in an environment with a temperature of -2°C and a pressure of 2000 bar;

[0036] (2) After the treated rice husk is fully steamed and sterilized in steam, it is dried to a water content of 72%, and after cooling down to normal temperature, 12 parts of glucose, 0.015 part of ferrous sulfate, 0.022 part of thiamine, 0.013 part of riboflavin, 0.012 part of nicotinic acid, 0.0103 part of dopamine hydrochloride, 0.0103 part of sodium iodide and mix well;

[0037] (3) Inoculate cellulase into the rice husk, the inoculation ratio is 5‰, enzymatic hydrolysis at 38°C, and the enzymatic hydrolysis time is 40 hours;

[0038] (4) Mix the rice husk obtained by enzymatic hydrolysis with 5 times the volume of water evenly, introduce it into a high-speed centrifuge, and heat the surface of the centrifuge at the same ...

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PUM

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Abstract

The invention relates to the field of oligosaccharide preparation, in particular to a preparation method of rice husk oligosaccharide. The method comprises the following steps that rice husk is crushed and is subjected to low-temperature high-pressure treatment; after full steaming and sterilization, drying is performed; glucose, ferrous sulfate, thiamine, riboflavin, niacin, dopamine hydrochloride and sodium iodide are added and uniformly stirred; cellulase is inoculated for enzymolysis; the mixture and water are uniformly mixed; high-speed centrifugation is performed; the mixed materials obtained through centrifugation are fed into a centrifugal dehydrator to be dehydrated; liquid obtained through dehydration is collected; vacuum concentration, purification and vacuum drying are performed to obtain an oligosaccharide finished product. The yield of the finally obtained oligosaccharide finished product is higher than 18.2 percent; the content of isomaltose oligosaccharide in the obtained oligosaccharide finished product accounts for 62 percent or higher.

Description

technical field [0001] The invention relates to the field of oligosaccharide preparation, in particular to a preparation method of rice husk oligosaccharide. Background technique [0002] Oligosaccharides, also known as oligosaccharides, integrate nutrition, health care and diet therapy, and are widely used in food, health care products, beverages, medicines, feed additives and other fields. It is a new functional sugar source that replaces sucrose. There are two main types of oligosaccharides. One is maltose oligosaccharides, which are easy to digest, low sweetness, and low permeability. They can prolong energy supply time, enhance body endurance, and resist fatigue. and other functions, and the other is the isomaltooligosaccharide called "bifidus factor". This kind of sugar enters the large intestine as the proliferation factor of bifidobacteria, which can effectively promote the growth and reproduction of beneficial bacteria in the human body—bifidobacteria, and inhibit ...

Claims

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Application Information

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IPC IPC(8): C07H3/06C07H1/08C08B37/08
CPCC07H1/08C07H3/06C08B37/0003
Inventor 严晓武
Owner 合肥市晶谷米业有限公司
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