Compounded composition containing isolongifolenoneoximelactam and flutriafol as well as bactericide containing isolongifolenoneoximelactam and flutriafol
The technology of folinone oxime lactam and compound composition, which is applied in the field of pesticides, can solve the problems of unsatisfactory control effect and the like, and achieve the effects of good control effect, prolonging service life and long lasting effect.
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preparation Embodiment
[0043] For uniformity, the auxiliaries used in the following preparation examples all use abbreviations or commodity codes.
[0044] 1. Preparation of suspending agent
[0045] Mix the surfactant, antifreeze, thickener, surfactant, and water, mix evenly by high-speed shearing, add isolongifolenone oxime lactam, triconazole in turn, and grind the balls in the ball mill for 2~ 3 hours, made the suspension concentrate of bactericide of the present invention.
[0046]
[0047] 2. Preparation of wettable powder
[0048] The isolongifolenone oxime lactam, triadol, wetting and dispersing agent, white carbon black, and fillers are uniformly mixed, pulverized by a jet mill, and stirred for 30 minutes to obtain the wettable powder of the fungicide of the present invention.
[0049]
[0050] 3. Preparation of water dispersible granules
[0051] Mix isolongifolenone oxime lactam, triconazole, wetting and dispersing agent, white carbon black, disintegrating agent, binder, and filler...
Embodiment 1
[0069] The test refers to "Pesticide Bioassay Technology" (Edited by Chen Nianchun, published by Beijing Agricultural University Press) and "Pesticide Indoor Bioassay Test Guidelines NY / T1156.2-2006". In this test, the zone of inhibition method was used. On the aseptic operating table, pour the NA medium into the NA plate, and after drying, take 0.1ml of X. citri bacteria suspension and apply it evenly on the NA plate with a coating stick. After drying, punch a hole in the center of the plate with a hole puncher with a diameter of 7 mm, and then take 100 μl of the drug solution into the small hole. 5 replicates for each concentration. The treatment of adding sterile water to the small well was used as the blank control. After treatment, place them in an incubator at 28±0.5°C for sterile cultivation, and take them out after 2 days. The diameter of the inhibition zone (in millimeters) of each treatment was measured by the cross method, and the average value of the diameter of...
Embodiment 2
[0075] The bacterial suspension concentration was 10 8 cfu mL -1 Add 0.5mL of pathogenic bacteria to each sterilized petri dish with a diameter of 9cm, then pour 15mL into gravy peptone medium cooled to 45°C, mix well, and solidify. At the bottom of the petri dish, mark the three corner positions of the regular triangle at an equidistant distance of 2.5 cm from the center, prevent the Oxford cup (10 mm in height, 6 mm in inner diameter), drop the same amount of different concentrations of the drug dilution solution, and store it under constant temperature and sterile conditions at 28 ° C. After culturing for 7 days, the diameter of the inhibition zone was measured, and the average value of the diameter of the inhibition zone and the inhibition rate were calculated. Use DPS data processing software for statistical analysis, and calculate the EC of each drug 50 , and then calculate the co-toxicity coefficient (CTC) according to Sun Yunpei's method.
[0076] The results of the...
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