A three-in-one test card for simultaneously detecting uric acid, creatinine, and urea in a sample and its preparation method
A three-in-one, in-sample technology, applied in the field of medical testing, can solve problems such as difficulty in realizing large-scale structure and formula, inconvenience for users or patients, and complicated operation, and achieve the effects of average flow rate, simple use, and uniform distribution
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[0057] A method for preparing a three-in-one test card for simultaneously detecting uric acid, creatinine, and urea in a sample, comprising the following steps:
[0058] Prepare uric acid reaction solution, the formula of uric acid reaction solution includes: 5-50KU / L urate oxidase, 1-20KU / L ascorbate oxidase, 1-20KU / L peroxidase, 0.1-10g / L film-forming agent, 10 -100g / L stabilizer, 0.1-10g / L surfactant, 0.1-10g / L chromogenic substance, 0.1-1M buffer; stir for 1 hour before use;
[0059] Preparation of creatinine reaction solution includes: 5-50KU / L creatinase, 5-100KU / L sarcosine oxidase, 5-100KU / L creatine hydrolase, 1-20KU / L ascorbate oxidase, 1-20KU / L over Oxidase, 0.1-10g / L film-forming agent, 10-100g / L stabilizer, 0.1-10g / L surfactant, 0.1-10g / L chromogenic substance, 0.1-1M buffer solution; use;
[0060] The preparation of urea reaction solution includes: 5-100KU / L urease, 0.1-10g / L film-forming agent, 10-100g / L stabilizer, 0.1-10g / L surfactant, 0.1-10g / L chromogenic ...
Embodiment 1
[0068] The preparation method of finished product 1 comprises the following steps:
[0069] Step 1, prepare uric acid reaction solution: mix 10KU uric acid oxidase, 3KU ascorbate oxidase, 1KU peroxidase, 0.5g polyvinyl alcohol, 10g bovine serum albumin, 3g trehalose, 0.5gtritonX-405, 1g N-ethyl-N-(2-hydroxy-3-sulfopropyl)-3,5-dimethylaniline sodium salt, 2g of 4-aminoantipyrine was added to 1L of 0.1MPH phosphate buffer solution with a pH value of 7.2 Stir in medium for one hour and set aside;
[0070] .Step 2, preparation of creatinine reaction solution: 10KU creatinase, 200KU sarcosine oxidase, 10KU creatine hydrolase, 2KU ascorbate oxidase, 1KU peroxidase, 0.5g polyvinyl alcohol, 10g bovine serum white Egg white, 3g treacle sugar, 0.5gtritonX-405, 1g N-ethyl-N-(2-hydroxy-3-sulfopropyl)-3,5-dimethylaniline sodium salt, 2g 4-aminoantipyrine Add it to 1L of 0.1MPH phosphate buffer solution with a pH value of 7.2 and stir for one hour before use;
[0071] .Step 3, prepare ur...
Embodiment 3
[0085] The manufacturing method of finished product 3 comprises the following steps:
[0086] Step 1, prepare uric acid reaction solution: mix 40KU uric acid oxidase, 15KU ascorbate oxidase, 10KU peroxidase, 5g polyvinyl alcohol, 50g bovine serum albumin, 50g treparin, 5gtritonX-405, 5g N- Ethyl-N-(2-hydroxy-3-sulfopropyl)-3,5-dimethylaniline sodium salt, 5g of 4-aminoantipyrine was added to 1L of 0.1MPH phosphate buffer with a value of 7.2 and stirred Standby in one hour;
[0087] .Step 2, preparation of creatinine reaction solution: 40KU creatinase, 40KU sarcosine oxidase, 50KU creatine hydrolase, 10KU ascorbate oxidase, 5KU peroxidase, 5g polyvinyl alcohol, 50g bovine serum albumin ,50g sea bath sugar, 5gtritonX-405, 5g N-ethyl-N-(2-hydroxy-3-sulfopropyl)-3,5-dimethylaniline sodium salt, 5g4-aminoantipyrine was added to 1L of 0.1MPH phosphate buffer solution with a pH value of 7.2 was stirred for one hour before use;
[0088] .Step 3, prepare urea reaction solution: 50KU...
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