2-methyl-4-chlorophenoxyacetic acid preparation method
A technology of methylphenoxyacetic acid sodium salt and chlorophenoxyacetic acid, which is applied in the field of preparation of 2-methyl-4-chlorophenoxyacetic acid, can solve the problems of increasing the production cost of dimethyl tetrachloride, lack of sodium chloroacetate, and reaction Fast speed and other problems, to achieve the effect of resource utilization, reduction of raw material costs, and reduction of energy consumption
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Embodiment 1
[0050] In the present embodiment, the original drug of dimethyltetrachloride is prepared by the following preparation method, including the following steps:
[0051] (1) Preparation of sodium chloroacetate aqueous solution: at 20-25°C, dissolve chloroacetic acid (content 99.5%, 838.8kg, 8.83kmol) in water (640kg); then control the system temperature at 20-30°C, and gradually add NaOH solution (content 30.2%, 1170kg, equivalent to NaOH is 8.83kmol), after adding in 2 hours, continue to stir and react for 10 minutes to make sodium chloroacetate aqueous solution for later use;
[0052] (2) Preparation of o-cresol sodium aqueous solution: first add sodium hydroxide solution (content 30.2%, 1170kg, 8.83kmol) in the reactor, then add o-cresol (content 99.0%, 955.6kg, 8.76kmol) , by controlling the addition rate of o-cresol to use the heat generated by the salt-forming reaction to maintain the temperature of the reaction system between 35-55°C, the addition is completed in 2 hours, a...
Embodiment 2
[0056] In the present embodiment, the original drug of dimethyltetrachloride is prepared by the following preparation method, including the following steps:
[0057] (1) Preparation of sodium chloroacetate aqueous solution: at 20-25°C, dissolve chloroacetic acid (content 99.5%, 838.8kg, 8.83kmol) in water (640kg); then control the system temperature at 20-30°C, and gradually add NaOH solution (content 30.2%, 1170kg, equivalent to NaOH is 8.83kmol), after adding in 2 hours, continue to stir and react for 10 minutes to make sodium chloroacetate aqueous solution for later use;
[0058] (2) Preparation of o-cresol sodium aqueous solution: first add sodium hydroxide solution (content 30.2%, 1170kg, 8.83kmol) in the reactor, then add o-cresol (content 99.0%, 955.6kg, 8.76kmol) , by controlling the addition rate of o-cresol to use the heat generated by the salt-forming reaction to maintain the temperature of the reaction system between 35-55°C, the addition is completed in 2 hours, a...
Embodiment 3
[0062] In the present embodiment, the original drug of dimethyltetrachloride is prepared by the following preparation method, including the following steps:
[0063] (1) Preparation of sodium chloroacetate aqueous solution: at 20-25°C, dissolve chloroacetic acid (content 99.5%, 838.8kg, 8.83kmol) in water (640kg); then control the system temperature at 20-30°C, and gradually add NaOH solution (content 30.2%, 1170kg, equivalent to NaOH is 8.83kmol), after adding in 2 hours, continue to stir and react for 10 minutes to make sodium chloroacetate aqueous solution for later use;
[0064] (2) Preparation of o-cresol sodium aqueous solution: first add sodium hydroxide solution (content 30.2%, 1170kg, 8.83kmol) in the reactor, then add o-cresol (content 99.0%, 955.6kg, 8.76kmol) , by controlling the addition rate of o-cresol to use the heat generated by the salt-forming reaction to maintain the temperature of the reaction system between 35-55°C, the addition is completed in 2 hours, a...
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