A heat-insulating and anti-cracking vertical barrier material for complex pollutants and its preparation method
A technology of anti-cracking and pollutants, which is applied in the field of isolation and control of contaminated sites, can solve the problems of barrier barrier failure, thermal diffusion, and increase in permeability coefficient, and achieve high thermal insulation function, good chemical compatibility, and enhanced treatment effect.
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Embodiment 1
[0054] Step 1) dissolving cetyltrimethylammonium bromide in distilled water, adding attapulgite, keeping the mass ratio of the two at 1:9, to obtain a suspension;
[0055] Step 2) Keep the suspension prepared in step 1) at a constant temperature at 30°C, use an electric mixer, keep the rotation speed at 200r / min, and continue stirring for 12h to obtain the suspension;
[0056] Step 3) Centrifuge the suspension prepared in step 2) at a speed of 2000r / min for 30min, pour out the supernatant, wash the residue with distilled water, and then centrifuge again. After repeating this operation 3 times, a solid product is obtained ;
[0057] Step 4) drying the solid product obtained in step 3) at 105° C. for 12 hours to obtain a sample;
[0058] Step 5) Grinding the dried sample in step 4) to 200 mesh to obtain an organically modified attapulgite, and then placing it in an oven at 60°C for later use;
[0059] Step 6) adding the treated organically modified attapulgite into the sodium-...
Embodiment 2
[0067] Step 1) dissolving cetyltrimethylammonium bromide in distilled water, adding attapulgite, keeping the mass ratio of the two at 1:9, to obtain a suspension;
[0068] Step 2) Keep the suspension prepared in step 1) at a constant temperature at 35°C, use an electric mixer, keep the rotation speed at 500r / min, and continue stirring for 24h to obtain the suspension;
[0069] Step 3) centrifuge the suspension prepared in step 2) at a speed of 4000r / min for 60min, pour out the supernatant, wash the residue with distilled water, and then centrifuge again. After repeating this operation 6 times, a solid product is obtained ;
[0070] Step 4) The solid product obtained in step 3) was dried at 105° C. for 24 hours to obtain a sample;
[0071] Step 5) Grinding the dried sample in step 4) to 300 mesh to obtain an organically modified attapulgite, and then placing it in an oven at 80° C. for subsequent use;
[0072] Step 6) adding the treated organically modified attapulgite into t...
Embodiment 3
[0080] Step 1) dissolving cetyltrimethylammonium bromide in distilled water, adding attapulgite, keeping the mass ratio of the two at 1:9, to obtain a suspension;
[0081] Step 2) Keep the suspension prepared in step 1) at a constant temperature at 30°C, use an electric mixer, keep the rotation speed at 200r / min, and continue stirring for 12h to obtain the suspension;
[0082] Step 3) Centrifuge the suspension prepared in step 2) at a speed of 2000r / min for 30min, pour out the supernatant, wash the residue with distilled water, and then centrifuge again. After repeating this operation 3 times, a solid product is obtained ;
[0083] Step 4) drying the solid product obtained in step 3) at 105° C. for 12 hours to obtain a sample;
[0084] Step 5) Grinding the dried sample in step 4) to 200 mesh to obtain an organically modified attapulgite, and then placing it in an oven at 60°C for later use;
[0085] Step 6) Add the treated organically modified attapulgite into the sodium-mod...
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