Phase-change temperature control material and preparation method thereof

A technology of phase change temperature control and phase change metal, which is applied in the direction of heat exchange materials, chemical instruments and methods, etc., can solve the problem of undeveloped phase change temperature control materials, organic phase change materials with small thermal conductivity, heat absorption or release Slow and other problems, to achieve the effect of large latent heat of phase change, increased interaction, and simple preparation method

Active Publication Date: 2020-12-25
GUANGZHOU UNIVERSITY
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, inorganic phase change materials are prone to phase separation when used in plastics, and are prone to irreversible dehydration during plastic extrusion and processing. In practical applications, the effect of phase change temperature control cannot be achieved, while the thermal conductivity of organic phase change materials Small, the energy storage capacity per unit volume is small, and the heat absorption or release is too slow. It is not conducive to temperature control when used in plastics, and it is easy to cause heat absorption too slow and cause a fire
Therefore, a phase change temperature control material with satisfactory practical effect has not been developed yet.

Method used

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  • Phase-change temperature control material and preparation method thereof
  • Phase-change temperature control material and preparation method thereof
  • Phase-change temperature control material and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0051] A phase change temperature control material, the composition of which is shown in the following table:

[0052] Table 1 Composition table of a phase change temperature control material

[0053] components parts by mass polycarbonate resin 75 Zirconia powder (particle size 2~10μm) 2 tris hydroxymethyl amino methane 8 Boron nitride powder (particle size 1~10μm) 8 Benzyltriethylammonium Chloride 2 ascorbic acid 1

[0054] The preparation method of the above-mentioned phase change temperature control material comprises the following steps: adding polycarbonate resin, zirconium dioxide powder, trimethylolaminomethane, boron nitride powder, benzyltriethylammonium chloride and ascorbic acid into the mixer, adjusting The speed of the mixer is 550r / min, stirring for 15min, and then transferred to the twin-screw extruder, the processing temperature is controlled at 215-230°C, the screw speed is 45-70r / min, extruded and granulated...

Embodiment 2

[0056] A phase change temperature control material, the composition of which is shown in the following table:

[0057] Table 2 Composition table of a phase change temperature control material

[0058]

[0059] The preparation method of the above-mentioned phase change temperature control material comprises the following steps: acrylonitrile-butadiene-styrene copolymer, copper oxide powder, isopropyl stearate, flake graphite powder, magnesium oxide powder, octadecyl diacetate Add methyl benzyl ammonium bromide, maleic anhydride grafted acrylonitrile-butadiene-styrene copolymer and p-tert-butylcatechol into the mixer, adjust the speed of the mixer to 600r / min, stir for 10min, and then transfer to double The screw extruder controls the processing temperature at 165-185°C and the screw speed at 55-80r / min, extrudes and granulates, and obtains the phase-change temperature-controlling material.

Embodiment 3

[0061] A phase change temperature control material, the composition of which is shown in the following table:

[0062] Table 3 Composition table of a phase change temperature control material

[0063] components parts by mass polyamide resin 90 Vanadium dioxide powder (particle size 2~10μm) 5 paraffin 10 Thermally conductive carbon powder (particle size 1~10μm) 7 Boron nitride powder (particle size 1~10μm) 5 Sodium Glycocholate 4 citric acid 0.3 Antioxidant 264 0.5

[0064] The preparation method of the above-mentioned phase change temperature control material comprises the following steps: adding polyamide resin, vanadium dioxide powder, paraffin wax, thermal conductive carbon powder, boron nitride powder, sodium glycocholate, citric acid and antioxidant 264 into the mixer, adjusting The speed of the mixer is 800r / min, stirring for 20min, and then transferred to the twin-screw extruder, the processing temperature is...

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Abstract

The invention discloses a phase-change temperature control material and a preparation method thereof. The phase-change temperature control material comprises the following components in parts by mass:70-100 parts of matrix resin; 1-10 parts of phase change metal oxide powder; 5-20 parts of an organic phase change material; 8-25 parts of heat conduction powder; 1-5 parts of a dispersing agent; 0-5parts of a compatilizer; and 0.1-1 part of antioxidant. The preparation method of the phase-change temperature control material comprises the following steps of: uniformly mixing the components, adding the mixture into a double-screw extruder, and carrying out extrusion granulation to obtain the phase-change temperature control material. The phase-change temperature control material has the advantages of high phase-change latent heat, high heat conductivity, excellent comprehensive mechanical properties and simple preparation method, and can be widely used for producing and processing batteryshells, household appliance shells, industrial equipment shells and other products.

Description

technical field [0001] The invention relates to the technical field of phase change materials, in particular to a phase change temperature control material and a preparation method thereof. Background technique [0002] Plastic is a material used in the production of many electronic and electrical equipment, such as: bases and protective covers of lamps, mobile phone and computer casings, battery casings, various home appliance components, etc. During the use of these devices, the temperature of the plastic shell is a major factor affecting the use effect. The control of the plastic temperature can ensure the stable output of electrical power and improve the user experience, and can effectively prevent the occurrence of fire. At present, the control of plastic temperature often requires additional refrigeration or heating, which consumes a lot of energy. Therefore, zero energy consumption temperature control has become the direction and focus of research. [0003] Phase ch...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C08L69/00C08K13/02C08K3/22C08K5/17C08K3/38C09K5/06C08L55/02C08K5/101C08K3/04C08L77/00C08L91/06C08L53/02C08L67/02
CPCC08K13/02C08K3/22C08K5/17C08K3/38C09K5/063C08L55/02C08L77/00C08L53/025C08K3/34C08K3/04C08K2201/005C08K2003/2244C08K2003/385C08L2205/025C08K2003/2248C08K2003/222C08K2201/014C08K2003/2289C08K2003/2296C08L2205/03C08K2003/2262C08K5/101C08K5/19C08L91/06C08L51/006C08K5/053C08K3/041C08K3/042C08L67/02Y02E60/14
Inventor 徐常威屈俊任
Owner GUANGZHOU UNIVERSITY
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