Fireproof adhesive, preparation method thereof and composite fireproof glass containing fireproof adhesive
A technology of fireproof glass and fireproof glue, applied in the field of fireproof glue, can solve the problems of UV radiation resistance, high temperature resistance, poor hardness and cold flow resistance, poor UV radiation resistance and high temperature resistance, and complex production process. and other problems, to achieve the effect of preventing heat conduction and radiation, good process control, and maintaining integrity
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[0075] One embodiment of the present invention also proposes a preparation method of fireproof glue, which specifically includes the following steps:
[0076] Add char-forming agent, char-forming aid, heat-resistant stabilizer, anti-condensation agent, ion fixative, storage stabilizer, defoamer and cross-linking agent in sequence to the nano-silica sol, stir while adding, and stir evenly After that, the first solution is obtained;
[0077] Add the water glass solution to the first solution, or add the first solution to the potassium water glass solution, transfer to a vacuum stirring tank, control the temperature of the system within 60°C, preferably 20-60°C, and stir for 30-60min, Then degassing under a vacuum lower than -0.096MPa for 30-40min, after depressurization, filter the solution with a 150-200 mesh screen to obtain a fireproof glue;
[0078] Among them, the raw materials in this method are the same as those of the above-mentioned fireproof glue. Specifically, in par...
Embodiment 1
[0122] A kind of fireproof glue, it is made of following raw material by weight: 25 parts of nano-silica sols with a mass concentration of 50%, 58 kg of potassium water glass solution with a mass concentration of 45%, 0.5 kg of sucrose, dihydrogen phosphate Potassium 0.1kg, boric acid 0.3kg, glycerol 15kg, starch 0.05kg, sodium polyphosphate 0.4kg, polyether modified silicone 0.5kg and sodium fluorosilicate 0.15kg.
[0123] The preparation method of the fireproof glue specifically includes the following steps: sequentially adding a char-forming agent, a char-forming aid, a heat-resistant stabilizer, an anti-condensation agent, an ion-fixing agent, a storage stabilizer, a defoamer and Cross-linking agent, stir evenly to obtain the first solution; mix potassium water glass solution with the first solution, stir at 40°C for 50 minutes, degas under -0.08MPa vacuum for 40 minutes, use 160-180 mesh sieve The net is filtered to obtain fireproof glue.
[0124] The method for preparin...
Embodiment 2
[0138] A kind of fireproof glue, by weight, it is made of the following raw materials: mass concentration is 48% nano-silica sol 23kg, mass concentration is 60kg of sodium water glass solution of 42%, fructose 0.3kg, potassium hydrogen phosphate 0.2 kg, borax 0.5kg, ethylene glycol 10kg, zinc oxide 0.1kg, potassium polyphosphate 0.5kg, polyoxyethylene polyoxypropylene pentaerythritol ether 0.2kg and aluminum fluoride 0.3kg.
[0139] The preparation method of the fireproof glue specifically includes the following steps: sequentially adding a char-forming agent, a char-forming aid, a heat-resistant stabilizer, an anti-condensation agent, an ion-fixing agent, a storage stabilizer, a defoamer and Cross-linking agent, stir evenly to obtain the first solution; mix potassium water glass solution with the first solution, stir at 60°C for 30 minutes, degas under -0.06MPa vacuum for 30 minutes, use 150-170 mesh sieve The net is filtered to obtain fireproof glue.
[0140] Adopt the same...
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