Powder activated carbon liquid in-situ regeneration method based on vacuum ultraviolet/chlorine/ultrasonic coupling effect
A powder activated carbon, vacuum ultraviolet technology, applied in separation methods, filter regeneration, chemical instruments and methods, etc., can solve the problems of high energy consumption, secondary pollution, large carbon loss, etc., to improve regeneration efficiency and reduce regeneration facilities. , strengthen the effect of desorption
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Embodiment 1
[0014] Embodiment 1: Add the regeneration solution of 0.05mM sodium hydroxide to the saturated powdered activated carbon concentrate that absorbs Rhodamine B at a concentration of 2000mg / L, and stir at 120rpm to form a powdered activated carbon mixed solution. Add 0.2mM sodium hypochlorite to the powdered activated carbon mixture, irradiate with vacuum ultraviolet rays with a power of 20W / L and a wavelength of 185mm, and at the same time act on ultrasonic waves with a frequency of 40kHz and a power of 90W / L for 30min, then separate and clean the regenerated powdered activated carbon , The obtained wet-type regenerated powdered activated carbon can be directly reused in the water treatment process. The adsorption capacity of the new carbon is 1360mg / g. After the regeneration treatment, the adsorption capacity of the powdered activated carbon is restored to 1156mg / g, and the regeneration rate reaches 85%.
Embodiment 2
[0015] Embodiment 2: Add the regeneration solution of 0.05mM hydrochloric acid in the saturated powdered activated carbon concentrate that absorbs aniline at a concentration of 5000mg / L, and continue stirring at 160rpm to form a powdered activated carbon mixed solution. Add 0.1mM ammonium chloride to the powdered activated carbon mixture, conduct 40kHz frequency, 180W / L power ultrasonic wave for 5 minutes, then increase 20W / L power, 185mm wavelength vacuum ultraviolet irradiation, and the combined action time of ultrasonic wave and vacuum ultraviolet light is 45min . Then the regenerated powdered activated carbon is separated and washed, and the obtained wet-type regenerated powdered activated carbon can be directly reused in the water treatment process. The adsorption capacity of the new carbon is 55.53mg / g. After the regeneration treatment, the adsorption capacity of the activated carbon is restored to 52.75mg / g g, the regeneration rate reaches 95%.
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