MPCVD equipment capable of realizing effective doping

A technology of equipment and pipelines, applied in the field of plasma chemical vapor deposition, can solve the problems such as the exploration, research and application realization of in-situ doping technology that restricts MPCVD, less attention to MPCVD research, impurity memory effect and contamination, etc. Doping contamination and memory effect, or the effect of overcoming doping contamination and memory effect and improving utilization

Active Publication Date: 2022-05-31
NANJING UNIV
View PDF14 Cites 0 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

For the growth of diamond single crystal films, a single reactant—methane is used in MPCVD, and there is no need for complex chemical reaction control. Researchers generally believe that microwave plasma, the source of reactive groups, is the most critical parameter affecting material growth. and most important conditions, therefore, less research attention has been paid to gas transport in MPCVD
[0004] However, the research on material doping is much more complicated. Studies have shown that the main reactive groups for the growth of diamond films are hydrogen atoms generated by high-temperature plasma and the reaction gas methane The molecular reaction leads to the single-carbon and double-carbon groups produced

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Image

Smart Image Click on the blue labels to locate them in the text.
Viewing Examples
Smart Image
  • MPCVD equipment capable of realizing effective doping
  • MPCVD equipment capable of realizing effective doping
  • MPCVD equipment capable of realizing effective doping

Examples

Experimental program
Comparison scheme
Effect test

Example Embodiment

Embodiment 1, second road gas transmission ring 4 are positioned at the annular gas transmission structure of support center

The influence of the formation of the body sphere 2 is reduced to a controllable range, a suitable structure is processed under the substrate support 5, and the second doping gas is mixed with the buffer.

The ring structure, that is, the gas transmission ring, can be made of stainless steel or metal molybdenum, or quartz suitable for microwave environments.

The influence of the formation of the body sphere 2 is reduced to a controllable range, a suitable structure is processed under the substrate support 5, and the second doping gas is mixed with the buffer.

The size of the jetting angle of the jetting hole on the above-mentioned circular ring structure is between 15 degrees and ‑15 degrees, so as to be conducive to controlling jetting

The situation of the distribution of the jet holes on the above-mentioned circular ring structure is evenly distrib...

Example Embodiment

Embodiment 2, the second road gas transmission ring 4 are positioned around the support, and keep the structure of a certain distance with the support

A circular ring is fixed around the substrate support, and its diameter is more than 6cm, and is suitable with the edge of the substrate support

The design and optimization of the second gas flow introduction structure that is fully compatible with the microwave coupling resonator is solved, and the reaction gas

is a metal such as stainless steel or molybdenum, as shown in Figure 3.

[0045] The height difference between the air jet holes on the above-mentioned circular ring structure and the support plane is between 0.5 centimeters to -0.5 centimeters,

The size of the jetting angle of the jetting hole on the above-mentioned circular ring structure is between 15 degrees and ‑15 degrees, so as to be conducive to controlling jetting

The situation of the distribution of the jet holes on the above-mentioned circular ring struct...

Example Embodiment

Embodiment 3, the second road gas transmission ring 4 are positioned around the support, and are in close contact with the structure of the support

A circular ring is fixed around the substrate support, and is kept in close contact with the edge of the substrate support to ensure that it is resistant to microwaves

The ring structure, that is, the gas transmission ring, can be made of stainless steel or metal molybdenum, or quartz suitable for microwave environments.

[0058] The height difference between the air jet holes on the above-mentioned circular ring structure and the support plane is between 0.5 centimeters to -0.5 centimeters,

The size of the jetting angle of the jetting hole on the above-mentioned circular ring structure is between 15 degrees and ‑15 degrees, so as to be conducive to controlling jetting

The situation of the distribution of the jet holes on the above-mentioned circular ring structure is evenly distributed along the circular ring with an angle, and...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

PUM

No PUM Login to view more

Abstract

An MPCVD device capable of achieving effective doping comprises a reaction chamber and a gas input structure, the gas input structure comprises two reaction gas pipelines, a distributor connected with the first pipeline evenly conveys gas into the reaction chamber, a gas outlet is located near the top of the reaction chamber, reaction gas is evenly conveyed into the reaction chamber, and the reaction gas is evenly conveyed into the reaction chamber. The gas distributor is located in the top area of the chamber; the first pipeline is used for transmitting a first reactant, the second pipeline is used for uniformly inputting doped reaction gas to the surface of a substrate through a circular ring gas distributor, the horizontal height of a gas transmission ring of the second pipeline is consistent with that of a substrate support, and the gas transmission ring can be placed at the central position and is of an inner concentric structure with the support; the gas transmission ring can also be placed on the periphery of the support, and the gas transmission ring and the support are of an outer concentric structure. According to the invention, the two pipelines are adopted to transmit the reaction gas respectively, so that the doping effect of MPCVD can be effectively realized.

Description

Technical field: [0001] The invention relates to the field of microwave plasma chemical vapor deposition, in particular to the gas input structure of equipment. Background technique: [0002] Microwave plasma chemical vapor deposition (MPCVD) is one of the mainstream techniques for epitaxy of diamond films, and is the best choice for preparing high-quality diamond films. The microwave resonant cavity and plasma ball in the MPCVD reaction chamber are the core of design and attention. After years of research and development, the use of MPCVD technology has been able to grow high-quality diamond single crystal thin film. [0003] In order to broaden the application fields of diamond and give full play to the advantages of diamond's physical and chemical properties, it is necessary to study the doping of diamond thin films. However, there is still a big gap between the research on diamond doping based on MPCVD technology and the single crystal growth technology. In addition to...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

Application Information

Patent Timeline
no application Login to view more
IPC IPC(8): C23C16/511C23C16/27C23C16/455C23C16/52C30B25/14C30B25/16C30B29/04
CPCC23C16/511C23C16/274C23C16/278C23C16/4558C23C16/279C30B25/16C30B25/14C30B29/04Y02P70/50C23C16/455C23C16/45502C23C16/24C23C16/45578C23C16/45561C23C16/4586
Inventor 顾书林刘松民朱顺明叶建东汤琨
Owner NANJING UNIV
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Try Eureka
PatSnap group products