Method for preparing iron ore concentrate by using microwave to deoxidize weak-magnetic iron minerals

A technology of weak magnetism and iron minerals, applied in chemical instruments and methods, magnetic separation, improvement of process efficiency, etc., can solve problems affecting microwave heating temperature rise rate and reduction reaction efficiency, large coke or charcoal consumption, high production cost, etc. , to achieve high reduction reaction efficiency and reduce energy consumption

Inactive Publication Date: 2007-08-08
WUHAN INSTITUTE OF TECHNOLOGY
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  • Summary
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  • Description
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  • Application Information

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Problems solved by technology

The existing problems are low heat exchange and mass transfer efficiency, high carbon consumption and high production cost
However, for low-grade iron ore, because it contains a large amount of gangue minerals that do not absorb microwaves, it will affect the heating rate of microwave heating and the reduction reaction efficiency. If the microwave carbon thermal reduction process is used, a large amount of coke or charcoal will be consumed, resulting in excessive cost high

Method used

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Examples

Experimental program
Comparison scheme
Effect test

example 1

[0024] Example 1: Pyrite slag after acid production by Hubei Chuxing Group. After analysis, the main chemical components are expressed in mass percentages: total iron (TFe) 40.24, S 1.12, P 0.07, Cu 0.32, FeO 6.99, SiO 2 14.72, CaO 4.62, MgO 0.68, among which iron minerals are mainly hematite. Mix the slag with 10% of the weight of the slag, put it into a microwave reduction roaster for reduction and roasting for 5 minutes, and then separate it with a permanent magnetic weak magnetic separator to obtain iron concentrate with a grade of 61.56%. The recovery rate is 86.13%.

example 2

[0025] Example 2: The red mud of Guangxi Pingguo Aluminum Plant contains hematite, goethite, hydrated garnet, diaspore, hydrous sodium aluminosilicate, perovskite, hydroxycalcite, calcite and other phases. Among them, the content of hematite and hydrated garnet is relatively high, and its main components are expressed in mass percentage: TFe 36.9, Al 2 o 3 15.06, SiO 2 10.16, Na 2 O 1.87, using strong magnetic separation process, the grade of iron ore concentrate is less than 55%, and the recovery rate is about 35%. Mix the red mud of Guangxi Pingguo Aluminum Plant with iron powder accounting for 12% of the weight of the red mud, put it in a microwave reduction roaster for 7 minutes, and then use a permanent magnetic weak magnetic separator to sort it, and the grade is 60.13%. The recovery rate of iron concentrate is 82.51%.

example 3

[0026] Example 3: Hubei Changyang Ningxiang type high phosphorus iron ore is an important iron ore that has not been developed and utilized in my country. The main mineral components of Hubei Changyang Ningxiang type sedimentary hematite are: hematite, siderite, calcite, white cloud Stone, chlorite, collophanite, pyrite, clay minerals and quartz, etc., mix Changyang pyrite containing 41.64% of TFe, P 1.02% and iron powder accounting for 10% of the weight of pyrite , placed in a microwave reduction roaster for reduction roasting for 5 minutes, and then sorted by a permanent magnet weak magnetic separator to obtain iron concentrate with a grade of 60.94%, a recovery rate of 83.79%, and iron concentrate with P≤0.25% dephosphorization effect.

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PUM

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Abstract

The invention discloses a making method of concentrate iron ore, which comprises the following steps: (1) adding 5-25% ferric powder or ferric mud into disposed powder evenly; (2) placing material into reducing sintering furnace to sinter for 2-8 min through microwave; reducing weak magnetic ferric ore into magnetic ferric ore; (3) proceeding magnetic cobbing to obtain the product.

Description

technical field [0001] The invention relates to a method for preparing iron concentrate by reducing weak magnetic iron minerals with microwaves from low-grade refractory iron oxide ores containing weak magnetic iron minerals and industrial wastes containing iron. Background technique [0002] my country's iron ore resources are mostly low-grade paragenetic iron ore, in which strong magnetic magnetite and weak magnetic hematite, limonite, siderite, and gangue minerals such as iron-containing silicate often co-exist together. In addition, in a large amount of iron-containing industrial waste, iron mainly exists in the form of weakly magnetic iron minerals, which is a valuable secondary iron ore resource. For example, my country discharges nearly 10 million tons of pyrite slag every year, which generally contains 30% to 50% iron; my country's alumina plants discharge more than 1.8 million tons of red mud every year, which contains 23% to 27% iron. If a large amount of iron-con...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C22B1/02B03C1/02
CPCY02P10/20
Inventor 张泽强胡文祥李冬莲
Owner WUHAN INSTITUTE OF TECHNOLOGY
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