Preparation method for hemp seed oil microcapsules

A technology of hemp seed oil and microcapsules, which is applied in the field of preparation of vegetable oil microcapsules, can solve the problems that linseed oil cannot be embedded and protected, the embedding rate is only 90%, and the temperature change is too complicated, etc., to achieve emulsion emulsification Good condition, good embedding effect, easy to obtain effect

Inactive Publication Date: 2015-04-29
INFINITUS (CHINA) CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

However, in the embedding process, the gum arabic powder needs to be dried in a drying oven to remove the oxidase, and the process is complicated; the embedding stage needs to use HAc to adjust the pH value to 3.0-3.5, and whether the change of the pH value has an impact on the microcapsule product cannot be determined. Conclusive, and the microcapsule emulsion needs to be maintained at 45~55°C during the embedding process. After adjusting the pH value, add distilled water, and the temperature should be lowered to 30~35°C, and then quickly add ice to bring the temperature down to 10°C. The change is too complicated; the drying method is dripping curing agent, natural precipitation, vacuum freeze-drying, high cost, long cycle, different degrees of agglomeration may occur, and poor fluidity
Chinese patent application CN102934703A "A Linseed Oil Microcapsule and Its Production Method" reports the preparation and production method of the linseed oil microcapsule, and its linseed oil load can reach 45%, and the embedding rate is ≥ 90%. , in its embodiment one, the drug loading is 19%, and the embedding rate can reach 95%; in the example three, the drug loading is 45%, and its embedding rate is reduced to 90%; it can be seen that with modified starch, maltodextrin and casein Although the embedding effect of sodium bicarbonate as a compound wall material is better, the embedding rate decreases rapidly with the increase of drug loading.
Although its drug loading can reach 45%, its embedding rate is only 90%, which cannot protect linseed oil well

Method used

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  • Preparation method for hemp seed oil microcapsules

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0046] (1) Prepare the wall material solution: use 49% maltodextrin, 22% modified starch, 10% gum arabic, 5% β-cyclodextrin and 14% sucrose as the wall material, add it to the batching tank at room temperature, and add water to prepare A wall material solution with a solids content of 43%.

[0047] (2) Sterilization: The wall material solution was sterilized in a 75°C water bath for 40 min.

[0048] (3) Emulsification: After cooling the sterilized wall material solution to 50°C, mix it with hemp seed oil, in which the mass ratio of wall material and hemp seed oil is 1:1.5, stir for 15 min to make it fully mixed , add water to form an emulsion with a solid content of 45%.

[0049] (4) High-pressure homogenization: Use a high-pressure homogenizer to homogenize the emulsion obtained in step (3) twice at a pressure of 20 MPa (200 bar) and three times at a pressure of 50 MPa (500 bar) to obtain a uniform Stable emulsion.

[0050] (5) Spray drying: Spray dry the emulsion obtained...

Embodiment 2

[0053] (1) Preparation of wall material solution: use 53% maltodextrin, 21% modified starch, 11% gum arabic, 5% β-cyclodextrin and 10% sucrose as wall materials, add them to the batching tank at room temperature, and add water to prepare A wall material solution with a solids content of 43%.

[0054] (2) Sterilization: The wall material solution was sterilized in a water bath at 85°C for 35 minutes.

[0055] (3) Emulsification: After cooling the sterilized wall material solution to 50°C, mix it with hemp seed oil, wherein the mass ratio of wall material and hemp seed oil is 1:1.25, and stir for 15 min to make it fully mixed , add water to form an emulsion with a solid content of 47%.

[0056] (4) High-pressure homogenization: Use a high-pressure homogenizer to homogenize the emulsion obtained in step (3) twice at a pressure of 25 MPa (250 bar), and then homogenize twice at a pressure of 55 MPa (550 bar) to obtain a homogeneous Stable emulsion.

[0057] (5) Spray drying: Spr...

Embodiment 3

[0060] (1) Prepare the wall material solution: use 57% maltodextrin, 21% modified starch, 10% gum arabic, 5% β-cyclodextrin and 6% sucrose as the wall material, add it to the batching tank at room temperature, and add water to prepare A wall material solution with a solids content of 43%.

[0061] (2) Sterilization: The wall material solution was sterilized in a 95°C water bath for 30 minutes.

[0062] (3) Emulsification: After cooling the sterilized wall material solution to 50°C, mix it with hemp seed oil, wherein the mass ratio of wall material and hemp seed oil is 1:1, stir for 15 min to make it fully mixed , add water to form an emulsion with a solid content of 50%.

[0063] (4) High-pressure homogenization: Use a high-pressure homogenizer to homogenize the emulsion obtained in step (3) twice at a pressure of 30MPa (300bar), and then homogenize twice at a pressure of 60MPa (600bar) to obtain a uniform and stable emulsion , 50 ℃ insulation 60min.

[0064] (5) Spray dryi...

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Abstract

The invention discloses a preparation method for hemp seed oil microcapsules. The preparation method comprises the following steps: (1) preparation of a wall material solution : taking maltodextrin, modified starch, Arabic gum and saccharose as main wall materials, and mixing the main wall materials and water to prepare the wall material solution; (2) sterilization: sterilizing the wall material solution; (3) emulsification: mixing and emulsifying the sterilized wall material solution and hemp seed oil to obtain an emulsion; (4) drying: spray-drying the emulsion to obtain the hemp seed oil microcapsules. The hemp seed oil microcapsules prepared by the method have the advantages of high oil content, high encapsulation rate, good stability and long quality guarantee period; the method is simple, lower in cost and conductive to practical production and application, and brings better economic benefits.

Description

technical field [0001] The invention relates to a preparation method of vegetable oil microcapsules, in particular to a preparation method of hemp seed oil microcapsules. Background technique [0002] Hemp is an annual Moraceae plant and one of the native plants in my country. As a precious "longevity hemp", hemp is rich in plant protein, lecithin, vitamin E, selenium, zinc, manganese, germanium and other essential trace elements for human body, and is also known as "plant brain". The a-linolenic acid in "gold" can inhibit allergies, anti-inflammatory and antibacterial, and has the effects of laxative, nourishing and tonifying. The oil content of hemp seeds is 30% to 35%, the oil content of hemp seeds is more than 50%, the unsaturated fatty acids in hemp seed oil account for more than 85% of the total fatty acids, and the vitamin E content is also quite high, which has great development and utilization. value. [0003] As the extract of hemp seed, hemp seed oil has the ef...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): A23L1/29A23P1/04A23L33/00
Inventor 黎科亮葛亚中马忠华李惠森
Owner INFINITUS (CHINA) CO LTD
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