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Preparation method of novel fluorescent PVC wire/cable shield material

A wire and cable and sheath material technology, which is applied in the field of preparation of new fluorescent PVC wire and cable sheath materials, and can solve the problems that PVC cable sheath materials do not have fluorescent or luminescent properties, etc.

Active Publication Date: 2015-07-15
SHAOGUAN YINGTIAN ENVIRONMENT FRIENDLY MATERIAL CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, with the continuous advancement of science and technology, more and more wires and cables for special occasions appear on the market, and the requirements for the corresponding wire and cable sheath materials are also getting higher and higher. The required wire and cable are mainly used in outdoor advertisements, exterior decoration of vehicles and ships, instrument indication, safety sign indication, sporting goods, military equipment, etc. Common PVC wire and cable sheathing materials include the PVC cable sheathing materials prepared by the aforementioned invention. Have fluorescent or luminescent properties, so the above requirements cannot be met

Method used

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  • Preparation method of novel fluorescent PVC wire/cable shield material

Examples

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Effect test

Embodiment 1

[0025] A preparation method of a novel fluorescent PVC wire and cable sheath material, the steps are as follows:

[0026] (1) cerium chloride is dissolved in ethanol to obtain a cerium chloride solution, and o-phenanthroline is dissolved in ethanol to obtain an o-phenanthroline solution, and p-toluic acid and ethanol are heated and stirred until completely dissolved, and the heating temperature is 60°C, use ammonia water to adjust the pH value to 9 to obtain p-toluic acid solution, heat and stir the cerium chloride solution and o-phenanthroline solution together for 20 minutes, then add p-toluic acid solution, the heating temperature is 60°C, continue After stirring for 1.5 hours, let it stand for 20 hours, filter and wash with ethanol, place it in a vacuum drying oven at 90°C and dry to obtain a white powder, wherein the molar ratio of cerium chloride, o-phenanthroline, and p-toluic acid The ratio is 2:5:3. Dissolve the white powder in dimethyl fumarate, add distilled water u...

Embodiment 2

[0031] A preparation method of a novel fluorescent PVC wire and cable sheath material, the steps are as follows:

[0032] (1) cerium chloride is dissolved in ethanol to obtain a cerium chloride solution, and o-phenanthroline is dissolved in ethanol to obtain an o-phenanthroline solution, and p-toluic acid and ethanol are heated and stirred until completely dissolved, and the heating temperature is 60°C, use ammonia water to adjust the pH value to 9 to obtain p-toluic acid solution, heat and stir the cerium chloride solution and o-phenanthroline solution together for 20 minutes, then add p-toluic acid solution, the heating temperature is 60°C, continue After stirring for 1.5 hours, let it stand for 20 hours, filter and wash with ethanol, place it in a vacuum drying oven at 90°C and dry to obtain a white powder, wherein the molar ratio of cerium chloride, o-phenanthroline, and p-toluic acid The ratio is 2:5:3. Dissolve the white powder in dimethyl fumarate, add distilled water u...

Embodiment 3

[0037] A preparation method of a novel fluorescent PVC wire and cable sheath material, the steps are as follows:

[0038] (1) cerium chloride is dissolved in ethanol to obtain a cerium chloride solution, and o-phenanthroline is dissolved in ethanol to obtain an o-phenanthroline solution, and p-toluic acid and ethanol are heated and stirred until completely dissolved, and the heating temperature is 60°C, use ammonia water to adjust the pH value to 9 to obtain p-toluic acid solution, heat and stir the cerium chloride solution and o-phenanthroline solution together for 20 minutes, then add p-toluic acid solution, the heating temperature is 60°C, continue After stirring for 1.5 hours, let it stand for 20 hours, filter and wash with ethanol, place it in a vacuum drying oven at 90°C and dry to obtain a white powder, wherein the molar ratio of cerium chloride, o-phenanthroline, and p-toluic acid The ratio is 2:5:3. Dissolve the white powder in dimethyl fumarate, add distilled water u...

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Abstract

The invention provides a preparation method of a novel fluorescent PVC wire / cable shield material. The preparation method comprises the following steps: (1) heating and stirring a terbium chloride solution and a phenanthroline solution together, adding a p-toluic acid solution, further stirring, standing, filtering, washing, and drying to obtain white powder; dissolving the white powder in dimethyl fumarate, adding distilled water to form a suspension, then adding sodium chloride and stearic acid, stirring, taking out, filtering and drying to obtain fluorescent powder; (2) adding ACR to the fluorescent power, stirring and mixing, extruding, melt spinning to obtain fluorescent fibers; (3) adding PVC, nano-montmorillonite, a heat stabilizer, a plasticizer, calcium carbonate, a coupling agent and an antioxidant together into a high speed stirrer for stirring to obtain a mixed material; and (4) dissolving the mixed material into a solvent, adding the fluorescent fibers, uniformly stirring to obtain a prepreg, drying, transferring to a die, heating, pressurizing and insulating heat, and naturally cooling to room temperature to obtain the fluorescent PVC wire / cable shield material. The shield material prepared by the preparation method provided by the invention has a relatively good fluorescent performance.

Description

Technical field: [0001] The invention relates to a wire and cable sheathing material, in particular to a preparation method of a novel fluorescent PVC wire and cable sheathing material. Background technique: [0002] PVC is the English abbreviation of polyvinyl chloride (Polyvinyl chloride), which is the polymerization reaction of vinyl chloride monomer (VCM) in peroxide, azo compound and other initiators, or by free radical polymerization under the action of light and heat. The polymers formed by mechanism polymerization, vinyl chloride homopolymer and vinyl chloride copolymer are collectively called vinyl chloride resin, which is a non-crystalline material. In actual use, PVC materials are often added with stabilizers, lubricants, auxiliary processing agents, colorants, anti-impact agents and other additives, which have good processing performance, low manufacturing cost, corrosion resistance, insulation and other good characteristics, and are widely used. Among them One ...

Claims

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Application Information

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IPC IPC(8): C08L27/06C08L33/04C08K13/02C08K5/00C08K3/34C08K3/26C08K5/12D01F6/52D01F1/10H01B7/17
CPCC08K2201/011C08L27/06C08L2201/08C08L2203/202C08L2205/03C08L2205/16D01F1/10H01B3/443H01B7/18C08L33/04C08L91/06C08K13/02C08K3/346C08K2003/265C08K5/12C08K3/16
Inventor 陆志强
Owner SHAOGUAN YINGTIAN ENVIRONMENT FRIENDLY MATERIAL CO LTD
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