A nanoporous lithium titanate nitride nanowire/nanomembrane integrated material and its preparation method and application
A lithium titanate nitride, nanoporous technology, applied in nanotechnology, nanotechnology, hybrid/electric double-layer capacitor manufacturing, etc. Low, improved electrical conductivity, the effect of improving electron transport and ion transfer efficiency
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Embodiment 1
[0035] Preparation method: (for the process flow chart, see the appended figure 2 )
[0036] (1) Preparation of sodium titanate nanowire / nanofilm material by hydrothermal reaction method: put the metal titanium sheet into a sodium hydroxide solution of a certain concentration, perform hydrothermal reaction at a certain temperature, and first form a lithium titanate nanofilm, A lithium titanate nanowire array is then formed to prepare a sodium titanate nanowire / nano film material grown in situ on the titanium sheet.
[0037] (2) Preparation of amorphous phase lithium titanate nanowire / nanofilm material by ion exchange method: put sodium titanate nanowire / nanofilm material into a certain concentration of hydrochloric acid solution, and perform hydrogen ion exchange reaction for sodium ion at a certain temperature , to prepare titanate nanowire / nano-membrane material; then put titanate nano-wire / nano-membrane material into lithium hydroxide solution with a certain concentration...
Embodiment 2
[0049] Preparation method: (for the process flow chart, see the appended figure 2 )
[0050] (1) Preparation of sodium titanate nanowire / nanofilm material by hydrothermal reaction method: put the metal titanium sheet into a sodium hydroxide solution of a certain concentration, perform hydrothermal reaction at a certain temperature, and first form a lithium titanate nanofilm, A lithium titanate nanowire array is then formed to prepare a sodium titanate nanowire / nano film material grown in situ on the titanium sheet.
[0051] (2) Preparation of amorphous phase lithium titanate nanowire / nanofilm material by ion exchange method: put sodium titanate nanowire / nanofilm material into a certain concentration of hydrochloric acid solution, and perform hydrogen ion exchange reaction for sodium ion at a certain temperature , to prepare titanate nanowire / nano-membrane material; then put titanate nano-wire / nano-membrane material into lithium hydroxide solution with a certain concentration...
Embodiment 3
[0063] Preparation method: (for the process flow chart, see the appended figure 2 )
[0064] (1) Preparation of sodium titanate nanowire / nanofilm material by hydrothermal reaction method: put the metal titanium sheet into a sodium hydroxide solution of a certain concentration, perform hydrothermal reaction at a certain temperature, and first form a lithium titanate nanofilm, A lithium titanate nanowire array is then formed to prepare a sodium titanate nanowire / nano film material grown in situ on the titanium sheet.
[0065] (2) Preparation of amorphous phase lithium titanate nanowire / nanofilm material by ion exchange method: put sodium titanate nanowire / nanofilm material into a certain concentration of hydrochloric acid solution, and perform hydrogen ion exchange reaction for sodium ion at a certain temperature , to prepare titanate nanowire / nano-membrane material; then put titanate nano-wire / nano-membrane material into lithium hydroxide solution with a certain concentration...
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