Producing technology of high-precision diamond grinding disc using metal adhesive
A technology of metal bond and diamond grinding wheel, applied in metal processing equipment, manufacturing tools, grinding/polishing equipment, etc. Thermal oxidizability, low equipment cost, and strength-enhancing effect
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[0024] The preparation technology of high-precision metal bond diamond grinding wheel sheet, it comprises the following steps:
[0025] (1) Preparation of titanium dioxide sol; when preparing titanium dioxide sol, first dissolve butyl titanate in absolute ethanol under stirring, then add diethanolamine, after the solution is evenly mixed, add ethanol aqueous solution dropwise, continue stirring, and then Aging to obtain titanium dioxide sol; the ratio of butyl titanate, water, diethanolamine and ethanol in the titanium dioxide sol is 1:1:1:(25-28). The invention adopts butyl titanate as an organic precursor, takes ethanol as an organic solvent, and prepares titanium dioxide sol through alcoholysis, hydrolysis and polycondensation reactions.
[0026] (2) Prepare alumina sol; mix aluminum isopropoxide, nitric acid, and deionized water evenly, stir and reflux at 90°C for 10 hours, then let stand for 24 hours, and filter to obtain alumina sol, in which aluminum isopropoxide, nitri...
Embodiment 1
[0034]First dissolve butyl titanate in absolute ethanol under stirring, then add diethanolamine, after the solution is uniformly mixed, then add ethanol aqueous solution dropwise, continue stirring, and then age at room temperature for 1 hour to obtain titanium dioxide sol, in which butyl titanate The ratio of ester, water, diethanolamine, and ethanol is 1:1:1:25; at the same time, mix aluminum isopropoxide, nitric acid, and deionized water evenly, stir and reflux at 90°C for 10h, and then let stand for 24h , and filtered to obtain alumina sol, wherein the ratio of aluminum isopropoxide, nitric acid, and deionized water is: 1:0.2:90. At the same time, the diamond particles are first soaked with hydrochloric acid solution, then rinsed with deionized water until the pH value of the rinse solution is 7, and dried, then ultrasonically cleaned with acetone, then rinsed with deionized water and dried, and then the cleaned diamond Soak the particles in the above titanium dioxide sol,...
Embodiment 2
[0036] First dissolve butyl titanate in absolute ethanol under stirring, then add diethanolamine, after the solution is uniformly mixed, then add ethanol aqueous solution dropwise, continue stirring, and then age at room temperature for 1 hour to obtain titanium dioxide sol, in which butyl titanate The ratio of ester, water, diethanolamine, and ethanol is 1:1:1:26.5; at the same time, mix aluminum isopropoxide, nitric acid, and deionized water evenly, stir and reflux at 90°C for 10 hours, and then let it stand for 24 hours , and filtered to obtain alumina sol, wherein the ratio of aluminum isopropoxide, nitric acid, and deionized water is: 1:0.2:90. At the same time, the diamond particles are first soaked with hydrochloric acid solution, then rinsed with deionized water until the pH value of the rinse solution is 7, and dried, then ultrasonically cleaned with acetone, then rinsed with deionized water and dried, and then the cleaned diamond Soak the particles in the above titan...
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