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Preparation method of nickel-copper alloy sheet material

A thin plate material, nickel-copper alloy technology, applied in metal material coating process, vacuum evaporation plating, coating, etc., can solve the problems of high technical difficulty in rolling nickel-copper alloy, low production efficiency, and environmental pollution by nickel metal , to achieve the effects of low manufacturing cost, high work efficiency and high product yield

Active Publication Date: 2019-01-22
江苏华力金属材料有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

It can be seen that the technical difficulty of rolling nickel-copper alloy is high, and the yield and production efficiency are low.
Moreover, nickel-copper alloys are smelted in an atmospheric environment, and there are disadvantages such as nickel metal polluting the environment.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0015] Embodiment 1: The preparation method of nickel-copper alloy sheet material includes the following steps:

[0016] (1) Cleaning of the substrate: Select a pure copper tape with a thickness of 0.15mm as the substrate. In order to remove oil stains, first use a 3.5% sodium carbonate lye to clean for 15 minutes at a temperature of 65°C; then in order to remove the oxide scale Clean the substrate in 3.5% dilute sulfuric acid for 15 minutes; then put the substrate in acetone solution, ethanol solution and deionized water for 25 minutes in order to improve the surface activity of the substrate and dry it for use;

[0017] (2) Select target material: select pure Ni target material or high nickel content nickel-copper 60wt.% Ni alloy target material, set aside;

[0018] (3) Preparation of cladding sheet: the copper strip substrate cleaned in step (1) is placed on the substrate table of the magnetron sputtering equipment as an anode, and the Ni target material and high nickel content ni...

Embodiment 2

[0019] Embodiment 2: The preparation method of nickel-copper alloy sheet material includes the following steps:

[0020] (1) Cleaning of the substrate: select a pure copper tape with a thickness of 0.2mm as the substrate. In order to remove oil stains, first clean with a 4.5% sodium carbonate lye for 10 minutes at a temperature of 75°C during cleaning; Clean the substrate in 4.5% dilute sulfuric acid for 10 minutes; then put the substrate in acetone solution, ethanol solution and deionized water for 35 minutes to increase the surface activity of the substrate, and then dry it for use;

[0021] (2) Select target material: select pure Ni target material or high nickel content nickel-copper 70wt.% Ni alloy target material, stand by;

[0022] (3) Preparation of cladding sheet: the copper strip substrate cleaned in step (1) is placed on the substrate table of the magnetron sputtering equipment as an anode, and the Ni target material and high nickel content nickel in step (2) Copper 60~70...

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Abstract

The invention relates to a preparation method of a nickel-copper alloy sheet material. The preparation method comprises the following steps: (1) substrate cleaning to remove oil stains and oxide scales so as to enhance the substrate surface activity, and blow-drying for later use; (2) selecting targets; (3) preparing a coated sheet; and (4) dispersing the solid solution. According to the preparation method, the multi-target magnetron sputtering process is utilized to perform continuous sputtering on the multiple targets, and the deposited film can not be easily polluted, and has the advantages of high deposition power and high quality. In the preparation process, the substrate can be cleaned to enhance the adhesion force of the substrate, and after-treatment dispersion is carried out to homogenize the alloy. The method has the advantages of high deposition rate, controllable quality and high work efficiency, does not have the problems of nickel element oxidation, environment pollution, hazards to human safety and the like in the preparation process due to the complete vacuum conditions, and thus, is suitable for industrial popularization.

Description

Technical field [0001] The invention relates to the preparation of an alloy material, in particular to a preparation method of a nickel-copper alloy sheet material. Background technique [0002] Nickel-copper alloy is a typical precipitation-strengthened alloy. It has a series of advantages such as high elasticity, high strength, high conductivity, corrosion resistance, fatigue resistance, small elastic hysteresis, non-magnetic, and no sparks when impacted. It is widely used It has broad application prospects in the aerospace, aviation, electronics, communications, machinery, petroleum, chemical, automotive and home appliance industries. [0003] At present, nickel-copper alloy plate materials are basically prepared by rolling, mainly including semi-continuous casting ingot + milling skin + heating + rough rolling + quenching + secondary rolling + quenching + pickling + brushing + finishing rolling. . As the nickel-copper alloy ingot tends to secondarily segregate during crystall...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C23C14/35
CPCC23C14/165C23C14/35C23C14/562C23C14/5806
Inventor 李铮李鲁
Owner 江苏华力金属材料有限公司
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