Fracture-resistant refractory material and preparation process thereof
A refractory material and a preparation process technology, applied in the field of refractory materials, can solve the problems of poor mechanical toughness, reduce the service life of the refractory material, affect the thermal shock resistance, etc., and achieve a simple preparation method, easy production, and excellent thermal shock resistance. Effect
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Embodiment 1
[0029] A fracture-resistant refractory material, comprising the following raw materials in parts by weight: 100 parts of alumina-silicon oxide mixed powder, 8 parts of calcium oxide, 6 parts of magnesium oxide, 2 parts of manganese oxide, 3 parts of titanium oxide, and 1 part of niobium pentoxide part, 10 parts of toughening fiber; in the alumina-silica mixed powder, the silica is 30mol%, and the alumina is 70mol%;
[0030] Wherein, the toughening fiber is a modified zirconia fiber, which is obtained through the following steps: 50 parts by weight of zirconia, after adding 3 parts by weight of calcium oxide and 1 part by weight of sodium oxide, and 400 parts by molar ratio of 1:1 The sodium chloride and potassium chloride compound salts were mixed and ground for 12 hours with absolute ethanol as the grinding medium, dried and calcined at 850°C for 6 hours, after calcined and cooled, ground, cleaned and dried.
[0031] A preparation process for a fracture-resistant refractory m...
Embodiment 2
[0036] A fracture-resistant refractory material, comprising the following raw materials in parts by weight: 100 parts of alumina-silicon oxide mixed powder, 9 parts of calcium oxide, 7 parts of magnesium oxide, 2.5 parts of manganese oxide, 3.5 parts of titanium oxide, and 1.5 parts of niobium pentoxide part, 12 parts of toughening fiber; in the alumina-silica mixed powder, the silica is 33mol%, and the alumina is 67mol%;
[0037] Wherein, the toughening fiber is a modified zirconia fiber, which is obtained through the following steps: 50 parts by weight of zirconia, after adding 3 parts by weight of calcium oxide and 1 part by weight of sodium oxide, and 400 parts by molar ratio of 1:1 The sodium chloride and potassium chloride compound salts were mixed and ground for 12 hours with absolute ethanol as the grinding medium, dried and calcined at 850°C for 6 hours, after calcined and cooled, ground, cleaned and dried.
[0038] A preparation process for a fracture-resistant refra...
Embodiment 3
[0043] A fracture-resistant refractory material, comprising the following raw materials in parts by weight: 100 parts of alumina-silicon oxide mixed powder, 10 parts of calcium oxide, 8 parts of magnesium oxide, 3 parts of manganese oxide, 4 parts of titanium oxide, and 2 parts of niobium pentoxide part, 15 parts of toughening fiber; in the alumina-silica mixed powder, the silica is 35mol%, and the alumina is 65mol%;
[0044] Wherein, the toughening fiber is a modified zirconia fiber, which is obtained through the following steps: 50 parts by weight of zirconia, after adding 3 parts by weight of calcium oxide and 1 part by weight of sodium oxide, and 400 parts by molar ratio of 1:1 The sodium chloride and potassium chloride compound salts were mixed and ground for 12 hours with absolute ethanol as the grinding medium, dried and calcined at 850°C for 6 hours, after calcined and cooled, ground, cleaned and dried.
[0045] A preparation process for a fracture-resistant refractory m...
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