Looking for breakthrough ideas for innovation challenges? Try Patsnap Eureka!

A preparing method of a polypyrrole magnetic conductive composite material

A conductive composite material, polypyridine technology, applied in the field of materials, can solve the problems of difficult to improve the agglomeration of inorganic fillers, hinder the application of conductive high-fraction materials, reduce the stability of finished products, etc., achieve good magnetic properties, enhance functionality, and improve stability. The effect of sexual intensity

Inactive Publication Date: 2017-09-26
张娟
View PDF5 Cites 2 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

This is mainly due to its poor processability and low stability, which seriously hinders the industrial application of conductive high-resolution materials.
Especially in the application of electrical components, conductive materials need to have good strength and stability, otherwise, no matter how good other properties are, they cannot be applied;
[0003] Application number: 201610885928.1 discloses a conductive coating for doors, including 45-55 parts of polyaniline, 18-20 parts of polypyrrole, 25-40 parts of carbon fiber, 7-12 parts of petroleum coke, 8-16 parts of silicon carbide, and 20 parts of graphite -25 parts, 6-9 parts of silver powder, 7-11 parts of nickel powder, 20-22 parts of single-walled carbon nanotubes, 36-40 parts of tin oxide, 23-25 ​​parts of zinc oxide, 22-24 parts of sodium pyrophosphate, three 4-8 parts of ethylhexyl phosphoric acid, 16-20 parts of sodium hexametaphosphate, 7-9 parts of sodium carboxymethylcellulose, 11-15 parts of oxidized polyethylene wax, 3-5 parts of polyvinyl chloride resin, bismalay 12-16 parts of imide, 20-25 parts of ethyl acrylate, 6-10 parts of nitrocellulose and 13-16 parts of terpineol, which are pre-mixed polypyrrole and single-walled carbon nanotubes, and then passed six Dispersion of sodium metaphosphate, sodium carboxymethyl cellulose, etc. to improve the compatibility of inorganic fillers such as single-walled carbon nanotubes between polymers; but this inorganic dispersion method is difficult to improve the agglomeration of inorganic fillers, easy Reduce the stability of the finished product

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0016] A preparation method of polypyrrole magnetoconductive composite material, comprising the following steps:

[0017] (1) Take ferrocene, add it to deionized water 50 times its weight, add trimethylolpropane, raise the temperature to 50-60°C, add p-phenoxybenzoic acid, keep stirring for 2 hours, filter, Wash the precipitate with water and dry at room temperature to obtain iron carboxylate;

[0018] (2) Take pyrrole, add it to tetrahydrofuran which is 30 times its weight, stir evenly, put it into a constant temperature water bath at 60°C, add metal potassium, keep stirring for 30 minutes, discharge and cool, add p-toluenesulfonyl chloride, and magnetically stir After 20 hours, add the product to deionized water, stir evenly, let it stand for 10 hours, filter, wash the precipitate with water, and dry it under vacuum at 60-70°C for 1 hour to obtain sulfonylpyrrole;

[0019] (3) Mix the above carboxylated iron and sulfonylpyrrole, add to tetrahydrofuran which is 2-3 times the...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

PUM

No PUM Login to View More

Abstract

A preparing method of a polypyrrole magnetic conductive composite material is disclosed. According to the composite material, carbon nanotubes participate polymerization of a pyrrole monomer, thus effectively improving dispersibility of the carbon nanotubes among polymers, effectively reducing agglomeration and increasing stability and strength of a finished-product material. Added hydroxylated iron adopting ferrocene as a raw material endows the finished-product material with good magnetic performance, thus expanding the using range of the finished-product material and enhancing functions of the finished-product material.

Description

technical field [0001] The invention belongs to the field of materials, and in particular relates to a preparation method of a polypyrrole magnetoconductive composite material. Background technique [0002] Conductive polymer materials are polymer materials with conductive functions (including semiconductivity, metal conductivity and superconductivity) and conductivity above 10S / m. Polymer conductive materials have the characteristics of low density, easy processing, corrosion resistance, large-area film formation, and conductivity can be adjusted within a range of more than ten orders of magnitude. They can not only be used as substitutes for various metal materials and inorganic conductive materials , and has become an indispensable class of materials in many advanced industrial sectors and cutting-edge technology fields. After years of extensive research worldwide, the application of conductive polymers in new energy materials has achieved great development, but it is far...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

Application Information

Patent Timeline
no application Login to View More
Patent Type & Authority Applications(China)
IPC IPC(8): C08G73/06C08K9/04C08K3/08C08K9/06C08K7/24C08L79/04
CPCC08G73/0611C08K3/08C08K7/24C08K9/04C08K9/06C08K2003/0856C08K2201/001C08K2201/01C08K2201/011C08L79/04
Inventor 张娟
Owner 张娟
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Patsnap Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Patsnap Eureka Blog
Learn More
PatSnap group products