Treatment and purification method of dyeing wastewater produced by wood processing
A technology for dye wastewater and wood, which is applied in water/sewage treatment, chemical instruments and methods, adsorbed water/sewage treatment, etc., and can solve the problems of easy pollution, low reuse rate, and high treatment cost.
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Embodiment 1
[0020] A method for treating and purifying dye wastewater in wood processing. The prepared nano-particles of manganese tetroxide are grown and attached to the pores of active zeolite to obtain a composite material of porous doped rod-shaped nano manganese tetroxide. The dye wastewater is purified and processed, and the preparation method of the compound comprises the following steps:
[0021] (1) Mix and stir 0.15 mol of potassium permanganate and 30 ml of ethylene glycol for 15 minutes, the stirring speed is 360 rpm, adjust the pH value in the range of 7.8-8.0 with ammonia water, and add 1.2 ml of butyl titanate coupling agent , stirred and mixed evenly, placed in a high-pressure reaction kettle, set the reaction temperature to 150 ° C, the reaction time was 12 hours, after the reaction was finished, it was naturally cooled to room temperature, the supernatant was poured out, and the products were respectively used deionized water and anhydrous Ethanol was centrifuged and was...
Embodiment 2
[0031] A method for treating and purifying dye wastewater in wood processing. The prepared nano-particles of manganese tetroxide are grown and attached to the pores of active zeolite to obtain a composite material of porous doped rod-shaped nano manganese tetroxide. The dye wastewater is purified and processed, and the preparation method of the compound comprises the following steps:
[0032] (1) Mix and stir 0.18 moles of potassium permanganate and 33 ml of ethylene glycol for 18 minutes, the stirring speed is 380 rpm, adjust the pH value in the range of 7.8-8.0 with ammonia water, and add 1.3 ml of butyl titanate coupling agent , stirred and mixed evenly, placed in the autoclave, set the reaction temperature to 155 ° C, the reaction time was 13 hours, after the reaction was finished, it was naturally cooled to room temperature, the supernatant was poured out, and the products were respectively used deionized water and anhydrous Ethanol was centrifuged and washed 3 times each...
Embodiment 3
[0042] A method for treating and purifying dye wastewater in wood processing. The prepared nano-particles of manganese tetroxide are grown and attached to the pores of active zeolite to obtain a composite material of porous doped rod-shaped nano manganese tetroxide. The dye wastewater is purified and processed, and the preparation method of the compound comprises the following steps:
[0043] (1) Mix and stir 0.20 mol of potassium permanganate and 35 ml of ethylene glycol for 20 minutes. The stirring speed is 400 rpm. Use ammonia water to adjust the pH value in the range of 7.8-8.0, and add 1.5 ml of butyl titanate coupling agent. , stirred and mixed evenly, placed in the autoclave, the reaction temperature was set to 160 ° C, the reaction time was 15 hours, after the reaction was finished, it was naturally cooled to room temperature, the supernatant was poured out, and the products were respectively used deionized water and anhydrous Ethanol was centrifuged and washed 4 times...
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