Ion exchange resins and uses
An ion exchange resin, resin matrix technology, applied in chemical instruments and methods, other chemical processes, physical/chemical process catalysts, etc., can solve problems to be further improved, and achieve improved glass transition temperature, good heat resistance, The effect of high swelling resistance
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Embodiment 1
[0040] [Example 1] Preparation of ion exchange resin
[0041] Add 47.0 grams of styrene, 2.3 grams of divinylbenzene, 30 grams of polystyrene and 1.6 grams of benzoyl peroxide initiator in a 500 milliliter three-necked flask, stir and react for 1.5 hours at 60 ° C; then add 0.6 grams of multi-walled Carbon nanotubes, continue stirring for 1 hour for pre-polymerization. 260 mL of deionized water in which 2.0 g of gelatin had been dissolved was added. Adjust the stirring speed, and at the same time gradually raise the temperature to 80°C, and react for 5 hours; then raise the temperature to 90°C, react for 5 hours, and finally raise the temperature to 98°C, and react for 8 hours. After the reaction, pour out the upper liquid, wash it with hot water at 85°C for several times, then wash it with cold water for several times, then filter it, put it in an oven for drying at 80°C, and sieve it to collect the particle size within the range of 0.35-0.60mm Composite macroporous microsp...
Embodiment 2
[0047] [embodiment 2] ion exchange resin preparation
[0048] Add monomer mixture solution (60.0 gram styrene, 1.0 gram divinylbenzene, 60 gram polystyrene, 1.6 gram multi-walled carbon nanotubes and 1.0 gram benzoyl peroxide containing initiator in 500 milliliters of there-necked flasks, The solution was first stirred and reacted at 70°C for 0.5 hours), started the agitator, added a mixed solution of 200 ml of deionized water and 4 grams of polyvinyl alcohol, raised the temperature to 85°C, reacted for 3 hours, then raised the temperature to 90°C, and reacted for 9 hours , and finally raised the temperature to 100°C, and reacted for 10 hours. After the reaction, pour out the upper liquid, wash with 85°C hot water, then wash with cold water, then filter, put in an oven to dry at 80°C, sieve, and collect composite macropores with a particle size within the range of 0.35 to 0.60 mm Microsphere B1.
[0049] Chloromethylation of composite microspheres: in a 500-ml three-necked f...
Embodiment 3
[0054] [embodiment 3] preparation of ion exchange resin
[0055] Add monomer mixture solution (42.5 gram styrene, 2.5 gram divinylbenzene, 10 gram polystyrene, 0.1 gram multi-walled carbon nanotube and 2.0 gram benzoyl peroxide containing initiator in 500 milliliters of there-necked flasks, The solution was first stirred and reacted at 70°C for 1.5 hours), a mixed solution of 200 ml of deionized water and 4 grams of polyvinyl alcohol was added, the temperature was raised to 85°C, and the reaction was carried out for 3 hours, then the temperature was raised to 90°C, and the reaction was carried out for 9 hours, and finally the temperature was raised to 100°C, react for 10 hours. After the reaction, pour out the upper liquid, wash with 85°C hot water, then wash with cold water, then filter, put it in an oven to dry at 80°C, sieve, and collect composite macropores with a particle size within the range of 0.35 to 0.60 mm Microsphere C1.
[0056] Chloromethylation of composite mi...
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