Multifunctional separation sieve mesh preparation method

A multi-functional, separation screen technology, applied in the field of preparation of multi-functional separation screen, can solve the problems of cumbersome preparation process, high manufacturing cost, no antibacterial activity, etc., and achieve good antibacterial performance effect

Inactive Publication Date: 2019-12-31
佛山市南海区里水镇经济促进局 +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] Stainless steel screens and polyester screens are commonly used industrial separation materials, but due to the limitation of their surface wettability, these materials cannot be used for the separation of wastewater, especially for the separation of oily wastewater, and for heavy metal ions in oily wastewater can't be separated
Patent CN 107893128 A discloses a preparation method and application of a titanium dioxide / sulfonated graphene oxide / silver nanoparticle composite membrane. The patent uses titanium dioxide to form a rough structure, and sulfonated graphene oxide and silver nanoparticles form a composite membrane. The properties of super-oleophobic and super-hydrophobic under oil are suitable for the oil-water separation process, but the preparation process is very cumbersome, and dangerous substances such as concentrated nitric acid are used, and the manufacturing cost is high.
Patent CN 108671585 A discloses a method for preparing a super-hydrophilic net for oil-water separation. This filter net is formed by attaching Portland cement to the surface of the screen net, but it is resistant to n-hexane, tea oil, peanut oil and other oily substances. The recovery rate is only 94%, and there is still a lot of room for improvement, resulting in the need for other separation membranes for further separation in actual use
Patent CN 109603205 A discloses a preparation method of a stainless steel filter screen for oil-water separation, but the filter screen only has the function of oil-water separation, cannot absorb heavy metals and has no antibacterial activity

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0036] A preparation method of a multifunctional separation screen, comprising the steps of:

[0037] (1) Take a 6*6cm 300-mesh stainless steel screen for pre-treatment. The treatment method is as follows: first, the stainless steel screen is placed in a cleaning agent, ultrasonicated at 20°C for 15 minutes, then rinsed with ultrapure water for 5 minutes, and placed in a Dry at 60°C for later use; the cleaning agent is composed of: sodium dodecylbenzenesulfonate (2w / %), isomeric tridecyl alcohol ethoxylate (8w / %), triethanolamine (5w / %) , propylene glycol monomethyl ether (10w / %), sodium benzoate (0.5w / %), deionized water (balance).

[0038] (2) After pretreatment, immerse the substrate in the polymer coating aqueous solution for 10 minutes; the polymer coating solution consists of polyvinyl alcohol (2%), sodium polyaspartate (12%), hydrophilic nano Silicon dioxide (0.5%), deionized water (balance).

[0039] (3) After soaking for 10 minutes, lift it up vertically, hang the c...

Embodiment 2

[0043] A preparation method of a multifunctional separation screen, comprising the steps of:

[0044] (1) Take a 6*6cm 300-mesh polyester screen for pre-treatment. The treatment method is as follows: first, the polyester screen is placed in a cleaning agent, ultrasonicated at 20°C for 15 minutes, then rinsed with ultrapure water for 5 minutes, and placed in a Dry at 60°C for later use; the cleaning agent is composed of: sodium dodecylbenzenesulfonate (3w / %), isomeric tridecyl alcohol ethoxylate (9w / %), triethanolamine (5w / %) , propylene glycol monomethyl ether (11w / %), sodium benzoate (0.5w / %), deionized water (balance).

[0045] (2) After pretreatment, immerse the base material in the polymer coating aqueous solution for 10 minutes; the polymer coating solution consists of polyvinyl alcohol (2.5%), sodium polyaspartate (12%), hydrophilic nano Silicon dioxide (0.5%), deionized water (balance).

[0046] (3) Soak for 10 minutes, then lift it up vertically, hang the coated scre...

Embodiment 3

[0050] A preparation method of a multifunctional separation screen, comprising the steps of:

[0051] (1) Take a 6*6cm 400-mesh brass screen for pre-treatment. The treatment method is as follows: First, the brass screen is placed in a cleaning agent, ultrasonicated at 20°C for 20 minutes, then rinsed with ultra-pure water for 10 minutes, and Place it under the condition of 60°C and dry it for later use; the cleaning agent is composed of: sodium dodecylbenzenesulfonate (4w / %), isomeric tridecyl alcohol ethoxylate (9w / %), triethanolamine (6w / %) %), propylene glycol monomethyl ether (12w / %), sodium benzoate (0.75w / %), deionized water (balance).

[0052] (2) After pretreatment, immerse the base material in the aqueous polymer coating solution for 10 minutes; the polymer coating solution consists of polyvinyl alcohol (3%), sodium polyaspartate (14%), hydrophilic nano Silicon dioxide (1.0%), deionized water (balance).

[0053] (3) After soaking for 10 minutes, lift it up verticall...

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Abstract

The invention discloses a multifunctional separation sieve mesh preparation method, which comprises: S1, pre-treating, wherein a sieve mesh is placed and washed in a cleaning agent, rinsing is performed with ultrapure water, and drying is performed so as to be spare; S2, soaking the sieve mesh pretreated in the step S1 in a polymer coating solution; S3, hanging and drying the sieve mesh coated inthe step S2, and soaking in an acidic glutaraldehyde solution; S4, taking out the sieve mesh obtained in the step S3, drying, and soaking in an antibacterial surfactant solution; and S5, taking out the sieve mesh soaked in the step S4, and drying to obtain the super-hydrophilic and super-oleophobic sieve mesh. According to the invention, the prepared sieve mesh has super-hydrophilic and super-oleophobic performance, can effectively achieve oil-water separation, has multiple functional groups contained in the coating on the surface of the sieve mesh, has excellent oil-water separation performance, further has performances of heavy metal ion adsorbing, antibacterial property and the like, and has substantially expanded application range.

Description

technical field [0001] The invention relates to the technical field of oily wastewater treatment and screen material surface modification, and more specifically, relates to a preparation method of a multifunctional separation screen. Background technique [0002] Water resources are necessary resources for people's life and production activities. With the growth of population and the development of economy, people are facing increasingly severe water resource problems. Therefore, the recycling and reuse of sewage treatment has become one of the important ways to solve the problem of water resources. With the development of industrialization and urbanization, oily wastewater has become one of the important sources of sewage. Oily wastewater is not only a large amount, but also comes from a wide range of sources, including oil and gas field mining, metal surface cleaning, steel rolling waste liquid, food production, etc. will produce a variety of oily wastewater. These oily...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C02F1/40C02F1/28B01D17/022C02F101/20
CPCB01D17/02C02F1/28C02F1/40C02F2101/20
Inventor 曾晖李金辉李国滨
Owner 佛山市南海区里水镇经济促进局
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