Solvent type spraying photocuring antibacterial coating as well as preparation method and application thereof
An antibacterial coating and photocuring technology, which is applied in epoxy resin coatings, antifouling/underwater coatings, polyurea/polyurethane coatings, etc., can solve the problems of antibacterial effect failure and achieve synergistic, effective and durable antibacterial effects , the effect of improving compatibility
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[0045] The raw materials for the preparation of the prepolymer I, in parts by weight, include: 12.9-15.4 parts of choline chloride, 18.9-25.9 parts of diisocyanate, 0.06-0.1 part of the second catalyst, and 33-41 parts of the diluent; The diisocyanate is selected from at least one of isophorone diisocyanate, dicyclohexylmethane diisocyanate, toluene diisocyanate, hexamethylene diisocyanate, and diphenylmethane diisocyanate; the second catalyst is selected from organic bismuth , Organotin, organozinc, potassium iodide; the diluent is an acrylate reactive diluent; more preferably, the acrylate reactive diluent is selected from 1,6-hexanediol diacrylate , Tripropylene glycol diacrylate, neopentyl glycol diacrylate, 1,4-butanediol diacrylate, trimethylolpropane triacrylate, pentaerythritol tetraacrylate, ethoxylated trimethylolpropane One or more of acrylates.
[0046] The preparation method of the prepolymer I includes the following steps: adding choline chloride and diluent into t...
Example Embodiment
[0114] Example 1
[0115] Example 1 provides a solvent-based spraying light-curing antibacterial coating. The raw materials for the preparation of the antibacterial coating include the following components in terms of weight percentage: 10% butyl acetate, 20% ethyl acetate, and 6% dilute Propylene glycol diacrylate, 12% trimethylolpropane triacrylate, 20% urethane acrylate, 15% epoxy acrylate, 12% light-curing antibacterial resin, 2.5% initiator, 0.3% leveling agent, 2.2% propylene glycol Methyl ether acetate.
[0116] The polyurethane acrylate is selected from allnex group EBECRYL 246; the epoxy acrylate is selected from Changxing Chemical 621A-80; the photoinitiator is selected from BASF photoinitiator Irgacure 184; the leveling agent is selected From BYK-333 leveling agent;
[0117] The raw materials for preparing the photocurable antibacterial resin include: 56.7g prepolymer I, 89.4g prepolymer II, 104.2g hydroxyl-terminated polydimethylsiloxane (number average molecular weigh...
Example Embodiment
[0125] Example 2
[0126] The difference between Example 2 and Example 1 is that the preparation raw materials of the antibacterial coating include the following components in terms of weight percentage: 10% butyl acetate, 20% ethyl acetate, and 6% tripropylene glycol diacrylate , 10% trimethylolpropane triacrylate, 19% polyurethane acrylate, 15% epoxy acrylate, 18% light-curable antibacterial resin, 2.5% initiator, 0.3% leveling agent, 2.2% propylene glycol methyl ether acetate .
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