Boron carbonitride nanosheet as well as preparation method and application thereof
A technology of nitrides and nanosheets, applied in the field of nanomaterials, can solve the problems of not extensive sources, time-consuming, complicated operation of hydrothermal method, etc.
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[0050]Such as figure 1 Shown, the preparation method of boron carbon nitride nanosheet of the present invention comprises the steps:
[0051] (1), take boron source, carbon source and nitrogen source and mix, obtain mixed powder;
[0052] (2), the mixed powder is stirred and dried, and placed in a planetary ball mill for uniform grinding to obtain an amorphous phase precursor;
[0053] (3) The amorphous phase precursor is degassed in a tube furnace and heat-treated at 800-1200° C. to obtain treated boron carbon nitride nanosheets (ie, boron-nitrogen-carbon materials);
[0054] (4) The borocarbonitride nanosheets treated in step (3) are ball milled in a planetary ball mill, and then purified to obtain borocarbonitride nanosheets.
[0055] Wherein, in the step (1), the boron source, the carbon source and the nitrogen source are the element mass ratios of B, C and N being 1:(0.05-1):(0.05-1).
[0056] (carbon source)
[0057] In step (1), the carbon source is selected from on...
Embodiment 1
[0084] The preparation method of the boron carbon nitride nanosheet of the present embodiment comprises the following steps:
[0085] (1), after mixing 2.06g boric acid, 2g urea and 0.2g carbon black, obtain mixed powder;
[0086] (2) Dry the mixed powder in an oven at 70°C for 30 minutes, and place it in a planetary ball mill at a speed of 500rmp, turn it for 20 minutes, stop for 5 minutes, turn it for another 20 minutes, mix evenly, grind finely, and obtain an amorphous phase precursor;
[0087] (3), the amorphous phase precursor is carried out degassing treatment, in the N of 100mL / min 2 Heat treatment at 1100°C for 2 hours under the protection of air flow, and cool down;
[0088] (4), place the product of step (3) in the planetary ball mill with a rotating speed of 500rmp, turn for 20min, stop for 5min, then turn for 20min to mix evenly, and grind finely;
[0089] (5) acid treatment with 10 wt% hydrochloric acid solution at room temperature; washing with water and ethano...
Embodiment 2
[0091] The preparation method of the boron carbon nitride nanosheet of the present embodiment comprises the following steps:
[0092] (1), after mixing 2.06g boric acid, 2g urea and 0.2g carbon black, obtain mixed powder;
[0093] (2) Dry the mixed powder in an oven at 70°C for 30 minutes, and place it in a planetary ball mill at a speed of 500rmp, turn it for 20 minutes, stop for 5 minutes, turn it for another 20 minutes, mix evenly, grind finely, and obtain an amorphous phase precursor;
[0094] (3), the amorphous phase precursor is carried out degassing treatment, in the N of 100mL / min 2 Heat treatment at 900°C for 2 hours under the protection of air flow, and cool down;
[0095] (4), put the product of step (3) in the ball mill at a speed of 500rmp, turn for 20min, stop for 5min, then turn for 20min to mix evenly, and grind finely;
[0096] (5) acid treatment with 10 wt% hydrochloric acid solution at room temperature; washing with water and ethanol, ultrasonic stripping;...
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