A kind of polyester low elastic yarn and preparation method thereof
A technology of polyester low elastic yarn and raw yarn is applied in the field of polyester fiber, which can solve the problems of discomfort, poor hygroscopicity and stuffiness, and achieve the effect of promoting full reaction, improving performance and inhibiting degradation.
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Embodiment 1
[0051] A preparation method of polyester low elastic yarn, comprising the following steps:
[0052] Step 1) Preparation of modified polyester chips:
[0053] Step 1-1) add the terephthalic acid of 10kg, the ethylene glycol of 10kg, the 1,2-pentanediol of 5kg, the catalyzer of 1kg in the first reactor, stirring speed is 500r / min, stirs 10min, is heated to 260°C, react for 5h to obtain a mixture;
[0054] Step 1-2) in the second reaction kettle, add 1kg of N-methylol acrylamide, 0.8kg of 3-aminopropanesulfonic acid, 0.8kg of glutaric acid and mix, heat to 80 ° C, and keep the temperature for 2h to obtain modifier;
[0055] Step 1-3) The mixture of 15kg and the modifier of 6kg were added to the polycondensation reaction kettle, mixed, heated to 260°C, polycondensation was carried out under the condition of pressure 1400Pa, discharged, solidified at 280°C for 10min, pelletized , to obtain modified polyester chips;
[0056] Step 2) Preparation of pre-oriented filament yarn:
...
Embodiment 2
[0065] Compared with Example 1, the only difference is:
[0066] In step 1-1), the addition of terephthalic acid is 15kg, the addition of ethylene glycol is 18kg, the addition of 1,2-pentanediol is 10kg, and the addition of catalyst is 2.5kg, heated to 280 ℃, the reaction is 3h;
[0067] In step 1-2), the addition of N-methylol acrylamide is 1.5kg, the addition of 3-aminopropanesulfonic acid is 1.2kg, the addition of glutaric acid is 1.5kg, heated to 120 ° C, Keep warm for 1h;
[0068] In step 1-3), the addition of the mixture is 25kg, and the addition of the modifier is 12kg, heated to 270 ° C;
[0069] In step 2), heating to 130°C, crystallization time is 2h, continuing to heat to 150°C, and drying for 3h;
[0070] In step 3), the control temperature of the first hot box is 95°C, and the control temperature of the second hot box is 70°C;
[0071] In step 4-1), the amount of antistatic treatment agent added is 5kg, the amount of water added is 100kg, heated to 65°C, and k...
Embodiment 3
[0074] Compared with Example 1, the only difference is:
[0075] In step 1-1), the addition of terephthalic acid is 12kg, the addition of ethylene glycol is 14kg, the addition of 1,2-pentanediol is 7kg, the addition of catalyst is 2kg, heated to 270 ° C , the reaction is 4h;
[0076] In step 1-2), the addition of N-methylol acrylamide is 1.2kg, the addition of 3-aminopropanesulfonic acid is 1kg, and the addition of glutaric acid is 1.1kg, heated to 100 ° C, insulation 1.5h;
[0077] In step 1-3), the addition of mixture is 25kg, and the addition of modifier is 12kg;
[0078] In step 4-1), the addition amount of antistatic treatment agent is 3kg, the addition amount of water is 60kg, heated to 62°C, and kept for 22min.
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